2,5-二羟甲基四氢呋喃合成路线 (共 15 条)
反应条件
sodium periodate; ruthenium trichloride in tetrahydrofuran; dichloromethane T=0°C;
参考文献
Roth, Stefanie; Goehler, Sabrina; Cheng, Huan; Stark, Christian B. W.
European Journal of Organic Chemistry, 2005 , # 19 p. 4109 - 4118
反应条件
Raney Ni (W-5); hydrogen in ethanol T=100°C; P=91200 Torr;
参考文献
Naemura; Fukuda; Takahashi; Konishi; Hirose; Tobe
Tetrahedron Asymmetry, 1993 , vol. 4, # 5 p. 911 - 918
反应条件
diethyl ether; nickel T=160°C; P=102971 Torr; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 77, p. 393,395
Journal of the Chemical Society, , p. 1,3
反应条件
potassium permanganate; carbon dioxide in water; acetone T=-10°C; pH 6;
参考文献
Journal of the American Chemical Society, , vol. 103, # 4 p. 940 - 941
反应条件
lithium aluminium tetrahydride in diethyl ether 12 h; Heating;
参考文献
Nakazaki, Masao; Naemura, Koichiro; Makimura, Masaru; Matsuda, Atsushi; Kawano, Takaaki; Ohta, Yoshihiro
Journal of Organic Chemistry, 1982 , vol. 47, # 12 p. 2429 - 2435
反应条件
hydrogen; palladium on activated charcoal in water T=140°C; P=52504.2 Torr; 0.5 h;
参考文献
Schiavo, V.; Descotes, G.; Mentech, J.
Bulletin de la Societe Chimique de France, 1991 , # 5 p. 704 - 711
反应条件
ruthenium trichloride in tetrahydrofuran; dichloromethane; water T=0°C; Title compound not separated from byproducts.;
参考文献
Synthesis, , # 17 p. 2751 - 2754
反应条件
1: Raney nickel; methanol / 90 °C / 58840.6 Torr / Hydrogenation 2: lithium alanate; tetrahydrofuran View Scheme
参考文献
Journal of the American Chemical Society, , vol. 77, p. 393,395
反应条件
hydrogen; Ru-carbon in water T=140°C; P=52504.2 Torr; different temperatures, pressures, reaction times and concentrations of catalyst, other catalysts; Product distribution;
参考文献
Bulletin de la Societe Chimique de France, , # 5 p. 704 - 711
反应条件
1: 91 percent / diethyl ether 2: 80 percent / LiAlH4 / diethyl ether / 12 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 12 p. 2429 - 2435