2-叔丁基-异吲哚-1,3-二酮合成路线 （共 27 条）
反应条件
1: in N,N-dimethyl acetamide
T=20°C; 24 h;
2: in N,N-dimethyl acetamide; xylene
T=140°C; 48 h;
参考文献
Li, Xiuru; Zhan, Jie; Li, Yuesheng
Macromolecules, 2004 , vol. 37, # 20 p. 7584 - 7594
反应条件
tert.-butylhydroperoxide; copper(l) chloride in dichloromethane; water
T=50°C; 24 h; Sealed tube;
参考文献
Yan, Xiaoyu; Fang, Kun; Liu, Hailan; Xi, Chanjuan
Chemical Communications, 2013 , vol. 49, # 90 p. 10650 - 10652
反应条件
triethylamine in acetonitrile
0.166667 h;
参考文献
Kehler, Jan; Breuer, Eli
Synthesis, 1998 , # 10 p. 1419 - 1420
反应条件
chromium(VI) oxide; sulfuric acid in acetone
1 h; Ambient temperature;
参考文献
Nishio, Takehiko; Yamamoto, Hiroshi
Journal of Heterocyclic Chemistry, 1995 , vol. 32, # 3 p. 883 - 892
反应条件
toluene-4-sulfonic acid in toluene
4 h; Heating;
参考文献
Aguilar, Nuria; Moyano, Albert; Pericas, Miquel A.; Riera, Antoni
Synthesis, 1998 , # 3 p. 313 - 316
反应条件
1: dichloromethane / 3 h / 30 °C / |Inert atmosphere
2: perchloric acid; acetic anhydride / 2 h / 30 °C / |Inert atmosphere
3: triethylamine / diethyl ether / 0.5 h / |Inert atmosphere
4: cesium fluoride / acetonitrile / 2 h / 30 °C / |Inert atmosphere
View Scheme
参考文献
Kaicharla, Trinadh; Thangaraj, Manikandan; Biju, Akkattu T.
Organic Letters, 2014 , vol. 16, # 6 p. 1728 - 1731
反应条件
1: perchloric acid; acetic anhydride / 2 h / 30 °C / |Inert atmosphere
2: triethylamine / diethyl ether / 0.5 h / |Inert atmosphere
3: cesium fluoride / acetonitrile / 2 h / 30 °C / |Inert atmosphere
View Scheme
参考文献
Kaicharla, Trinadh; Thangaraj, Manikandan; Biju, Akkattu T.
Organic Letters, 2014 , vol. 16, # 6 p. 1728 - 1731
反应条件
30 min, 110 deg C; 1 h, 130 deg C; 3 h, 180 deg C;
参考文献
Kreher, Richard P.; Hennige, Hans; Jelitto, Frank; Preut, Johannes
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1989 , vol. 44, # 9 p. 1132 - 1148
反应条件
2,4,6-trichloro-1,3,5-triazine; C2F6NO4S2(1-)*C8H14N3O(1+) in acetonitrile
T=65°C; 3.4 h;
参考文献
Hullio, Ahmed Ali; Mastoi
Chinese Journal of Chemistry, 2012 , vol. 30, # 7 p. 1647 - 1657
参考文献
Ranadive, V. B.; Khadilkar, B. M.; Samant, S. D.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1994 , vol. 33, p. 1175 - 1177
