2',3'-O-异丙叉肌苷合成路线 (共 13 条)
反应条件
toluene-4-sulfonic acid in N,N-dimethyl-formamide 24 h; Inert atmosphere;
参考文献
Vertuani, Silvia; Baldisserotto, Anna; Varani, Katia; Borea, Pier Andrea; De Marcos Maria Cruz, Bonache; Ferraro, Luca; Manfredini, Stefano; Dalpiaz, Alessandro
European Journal of Medicinal Chemistry, 2012 , vol. 54, p. 202 - 209
反应条件
1: With perchloric acid T=20°C; 1.5 h; 2: With ammonia in water T=20°C; 3 h;
参考文献
Xu, Yanli; Jin, Hongwei; Yang, Zhenjun; Zhang, Liangren; Zhang, Lihe
Tetrahedron, 2009 , vol. 65, # 27 p. 5228 - 5239
反应条件
toluene-4-sulfonic acid in water; acetone T=20°C;
参考文献
Li, Xu; Tanner, Martin E.
Tetrahedron Letters, 2010 , vol. 51, # 49 p. 6463 - 6465
反应条件
methanol; water; triethylamine T=71°C; 1 h;
参考文献
Meier, Lidiane; Monteiro, Gustavo C.; Baldissera, Rodrigo A.M.; Sa, Marcus Mandolesi
Journal of the Brazilian Chemical Society, 2010 , vol. 21, # 5 p. 859 - 866
参考文献
Journal of Biological Chemistry, , vol. 111, p. 313,321,322
Journal of the Chemical Society, , p. 1348,1351
反应条件
adenosine deaminase EC 3.5.4.4 in phosphate buffer; dimethyl sulfoxide pH=7.4; Product distribution; Further Variations:pH-valuesReagents;
参考文献
Nucleosides, Nucleotides and Nucleic Acids, , vol. 26, # 1 p. 121 - 127
反应条件
1: 83 percent / 2,2,6,6-tetramethyl-1-piperidinyloxy free radical; iodosobenzene diacetate / acetonitrile; H2O / 4 h / 20 °C 2: SOCl2; DMF / CHCl3 / 5 h / Heating View Scheme
参考文献
Olsson; Kusachi; Thompson; Ukena; Padgett; Daly
Journal of medicinal chemistry, 1986 , vol. 29, # 9 p. 1683 - 1689
参考文献
Qu, Gui-Rong; Xia, Ran; Yang, Xi-Ning; Li, Jian-Guo; Wang, Dong-Chao; Guo, Hai-Ming
Journal of Organic Chemistry, 2008 , vol. 73, # 6 p. 2416 - 2419
反应条件
erbium(III) triflate in water T=120°C; 0.5 h; Microwave irradiation;
参考文献
Procopio, Antonio; Gaspari, Marco; Nardi, Monica; Oliverio, Manuela; Romeo, Roberto
Tetrahedron Letters, 2008 , vol. 49, # 12 p. 1961 - 1964
反应条件
1: 100 percent / RuCl3*3H2O, NaIO4 / H2O; acetonitrile; CCl4 / Ambient temperature 2: glacial acetic acid / H2O / Heating; pH 2.3-2.4 View Scheme
参考文献
Singh, Ambarish K.; Varma, Rajender S.
Tetrahedron Letters, 1992 , vol. 33, # 17 p. 2307 - 2310