3-甲基-2-环己烯-1-醇合成路线 （共 78 条）
反应条件
3-[{2-[4-(4-{2-[bis-(2-methoxycarbonyl-ethyl)-amino]-ethylcarbamoyl}-phenyldisulfanyl)-benzoylamino]-ethyl}-(2-methoxycarbonyl-ethyl)-amino]-propionic acid methyl ester in benzene T=20°C; 2.5 h; UV-irradiation;
参考文献
Heteroatom Chemistry, , vol. 20, # 1 p. 1 - 11
反应条件
hydrogen; 2,2'-dipyridylmethane-Pd(OAc)2 in dichloromethane P=760 Torr; Ambient temperaturevariation of catalysts and solvent; Product distribution;
参考文献
Moberg, Christina; Rakos, Laszlo
Journal of Organometallic Chemistry, 1987 , vol. 335, p. 125 - 132
反应条件
(8-oxyquinolinate)2VV(O)(OiPr); triethylamine in 1,2-dichloro-ethane T=80°C; 24 h;
参考文献
Hanson, Susan K.; Wu, Ruilian; Silks, L. A. Pete
Organic Letters, 2011 , vol. 13, # 8 p. 1908 - 1911
反应条件
Oxonereg;; (ethylenedinitrilo)tetraacetic acid disodium salt; sodium hydrogencarbonate; acetone in water; acetonitrile Ambient temperaturepH 7.0-7.5, other reagents: various ketones/Na2*EDTA/Oxone/NaHCO3, Na2*EDTA/Oxone/NaHCO3, m-chloroperbenzoic acid/NaHCO3;
参考文献
Yang, Dan; Jiao, Guan-Sheng; Yip, Yiu-Chung; Wong, Man-Kin
Journal of Organic Chemistry, 1999 , vol. 64, # 5 p. 1635 - 1639
反应条件
D-glucopyranose; nicotinamide adenine dinucleotide phosphate in aq. phosphate buffer T=25°C; pH=7.4; 21 h; stereoselective reaction;
参考文献
Roiban, Gheorghe-Doru; Agudo, Ruben; Reetz, Manfred T.
Tetrahedron, 2013 , vol. 69, # 26 p. 5306 - 5311
反应条件
D-glucopyranose; nicotinamide adenine dinucleotide phosphate in aq. phosphate buffer T=25°C; pH=7 - 8; 21 h; Enzymatic reaction; stereoselective reaction;
参考文献
Roiban, Gheorghe-Doru; Agudo, Ruben; Reetz, Manfred T.
Tetrahedron, 2013 , vol. 69, # 26 p. 5306 - 5311
反应条件
D-glucose; Yamadazyma farinosa IFO 10896 in phosphate buffer T=30°C; pH=6.5; 4 h;
参考文献
Chemistry Letters, , vol. 36, # 12 p. 1428 - 1429
反应条件
3-[{2-[4-(4-{2-[bis-(2-methoxycarbonyl-ethyl)-amino]-ethylcarbamoyl}-phenyldisulfanyl)-benzoylamino]-ethyl}-(2-methoxycarbonyl-ethyl)-amino]-propionic acid methyl ester in benzene T=20°C; 2.5 h; UV-irradiation;
参考文献
Heteroatom Chemistry, , vol. 20, # 1 p. 1 - 11
反应条件
3,3-dimethyldioxirane in acetone Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Murray, Robert W.; Singh, Megh; Williams, Brian L.; Moncrieff, Hazel M.
Journal of Organic Chemistry, 1996 , vol. 61, # 5 p. 1830 - 1841
反应条件
tert.-butylhydroperoxide; dimethyl(n-butyl)amine; zeolite 4 A; titanium silicalite in toluene T=59.85°C; Epoxidation; 0.25 h; Product distribution; Further Variations:Reagentstime;
参考文献
Dusi, Marco; Mallat, Tamas; Baiker, Alfons
Journal of Catalysis, 1999 , vol. 187, # 1 p. 191 - 201
