3-甲基-2-环己烯-1-醇合成路线 （共 78 条）
反应条件
potassium hydroxide; hydrogen; RuCl2lt;(R)-binapgt;(dmf)n*(R,R)-1,2-diphenylethylenediamine in isopropyl alcohol T=28°C; P=6080 Torr; 18 h;
参考文献
Ohkuma, Takeshi; Ikehira, Hideyuki; Ikariya, Takao; Noyori, Ryoji
Synlett, 1997 , # SPEC. ISS. p. 467 - 468
反应条件
tert.-butylhydroperoxide; [ruthenium(II)(terpy)(4′-methyl-2,2′-bipyridine-4-carboxylic acid)Cl]Cl in tert-butyl alcohol T=26°C; Inert atmosphere;
参考文献
Polyhedron, , vol. 52, p. 634 - 638
反应条件
lithium aluminium tetrahydride; 4,7,13,18-tetraoxa-1,10-diazabicyclo[8.5.5]eicosane in tetrahydrofuran 0.25 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 36, p. 1937 - 1942
反应条件
sodium tetrahydroborate in various solvent(s) T=20°C; 3 h;
参考文献
Synthetic Communications, , vol. 35, # 6 p. 867 - 872
反应条件
FeCl3(5-chlorobenzotriazole)2·2(5-chlorobenzotriazole); dihydrogen peroxide in water; acetonitrile T=26°C; 2 h; Inert atmosphere; Reagent/catalystTime;
参考文献
Polyhedron, , vol. 64, p. 189 - 202
反应条件
tert.-butyl lithium in diethyl ether; pentane 1. -78 deg C, 20 min 2. 0 deg C, 10 min;
参考文献
Wu, Kuo-Ming; Okamura, William H.
Journal of Organic Chemistry, 1990 , vol. 55, # 13 p. 4025 - 4033
反应条件
n-butyllithium in hexane T=-78 - -20°C; Wittig Rearrangement; 8 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 78, # 17 p. 8915 - 8921
反应条件
tetrabutyl ammonium fluoride in acetonitrile 1.5 h; Heating;
参考文献
Fristad, William E.; Bailey, Thomas R.; Paquette, Leo A.
Journal of Organic Chemistry, 1980 , vol. 45, # 15 p. 3028 - 3037
反应条件
sodium tetrahydroborate; non ionic glycosidic surfactant in water 12 h; Ambient temperature;
参考文献
Tetrahedron Letters, , vol. 37, # 1 p. 53 - 56
反应条件
sec.-butyllithium in tetrahydrofuran T=-78°C; 4 h; Inert atmosphere; Reagent/catalyst;
参考文献
Hanessian, Stephen; Dorich, Stephane; Chattopadhyay, Amit Kumar; Bueschleb, Martin
Journal of Organic Chemistry, 2013 , vol. 78, # 17 p. 8915 - 8921
