1-溴-2-苯基乙炔-苯合成路线 （共 49 条）
反应条件
copper(l) iodide; Pd2(PPh3)2Cl2; triethylamine T=20°C; Inert atmosphere;
参考文献
Ishida, Tomonobu; Kikuchi, Satoshi; Tsubo, Tatsuyuki; Yamada, Tohru
Organic Letters, 2013 , vol. 15, # 4 p. 848 - 851
反应条件
1,1'-bis-(diphenylphosphino)ferrocene; copper(l) iodide; palladium diacetate; triethylamine in N,N-dimethyl-formamide T=20°C; Sonogashira coupling; Inert atmosphere;
参考文献
Prakash, Anjanappa; Dibakar, Mullick; Selvakumar, Kumaravel; Ruckmani, Kandasamy; Sivakumar, Manickam
Tetrahedron Letters, 2011 , vol. 52, # 43 p. 5625 - 5628
反应条件
dichlorolt;(2-dimethylamino)propyldiphenylphosphinegt;palladium; lithium bromide in diethyl ether; toluene T=20°C; 4 h;
参考文献
Kamikawa, Takashi; Hayashi, Tamio
Journal of Organic Chemistry, 1998 , vol. 63, # 24 p. 8922 - 8925
反应条件
potassium fluoride; 18-crown-6 ether; copper(ll) bromide in ethylene glycol dimethyl ether T=80°C; 21 h;
参考文献
Morishita, Takami; Yoshida, Hiroto; Ohshita, Joji
Chemical Communications, 2010 , vol. 46, # 4 p. 640 - 642
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=20°C; 1 h;
参考文献
Okano, Masateru; Amano, Masayuki; Takagi, Kentaro
Tetrahedron Letters, 1998 , vol. 39, # 19 p. 3001 - 3004
反应条件
potassium fluoride; 18-crown-6 ether; copper(ll) bromide in ethylene glycol dimethyl ether T=25°C; 17 h;
参考文献
Morishita, Takami; Yoshida, Hiroto; Ohshita, Joji
Chemical Communications, 2010 , vol. 46, # 4 p. 640 - 642
反应条件
bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; tetra-(n-butyl)ammonium iodide; diethylamine in acetonitrile T=20°C; Sonogashira coupling; 2 h; Inert atmosphere;
参考文献
Fabrizi, Giancarlo; Goggiamani, Antonella; Sferrazza, Alessio; Cacchi, Sandro
Angewandte Chemie - International Edition, 2010 , vol. 49, # 24 p. 4067 - 4070
反应条件
KOC(O)Ph; triphenylphosphine; copper(l) chloride in 1,3-dimethyl-imidazolidin-2-one T=120°C; Sila-Sonogashira-Hagihara cross-coupling reaction; 12 h; Inert atmosphere;
参考文献
Ihara, Hideki; Ueda, Akinori; Suginome, Michinori
Chemistry Letters, 2011 , vol. 40, # 9 p. 972 - 974
反应条件
triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran; diethyl ether; hexane T=75°C;
参考文献
John, Jens A.; Tour, James M.
Tetrahedron, 1997 , vol. 53, # 45 p. 15515 - 15534
反应条件
pyrrolidine; triphenylphosphine; 1-n-butyl-3-methylimidazolium hexafluorophosphate; bis(η3-allyl-μ-chloropalladium(II)) T=130°C; Heck alkynylation; 24 h;
参考文献
Hierso, Jean-Cyrille; Boudon, Julien; Picquet, Michel; Meunier, Philippe
European Journal of Organic Chemistry, 2007 , # 4 p. 583 - 587
