1-硝基-4-硫氰酸基苯合成路线 (共 52 条)
反应条件
1: HNO3+H2SO4 / 90 °C 2: aniline; alcohol View Scheme
参考文献
Challenger; Collins
Journal of the Chemical Society, 1924 , vol. 125, p. 1379
反应条件
1,10-phenanthroline; Cu(BF4)2; [Cu(CH3CN)4]BF4 in acetonitrile
T=0 - 5°C;
参考文献
Beletskaya, Irina P.; Sigeev, Alexander S.; Peregudov, Alexander S.; Petrovskii, Pavel V.
Mendeleev Communications, 2006 , # 5 p. 250 - 251
反应条件
in acetonitrile
T=20 - 25°C; 0.5 h;
参考文献
Barbero; Degani; Diulgheroff; Dughera; Fochi
Synthesis, 2001 , # 4 p. 585 - 590
反应条件
potassium carbonate in tetrahydrofuran
1 h; Heating;
参考文献
Harusawa, Shinya; Shioiri, Takayuki
Tetrahedron Letters, 1982 , vol. 23, # 4 p. 447 - 448
反应条件
4-methylpyridine; oxygen; copper diacetate in acetonitrile
T=80°C; P=1500.15 Torr; 12 h; AutoclaveMolecular sieve;
参考文献
Sun, Nan; Zhang, Han; Mo, Weimin; Hu, Baoxiang; Shen, Zhenlu; Hu, Xinquan
Synlett, 2013 , vol. 24, # 11 art. no. ST-2013-W0236-L, p. 1443 - 1447
反应条件
in acetonitrile
Ambient temperature;
参考文献
Abramovitch, Rudolph A.; Miller, Adrian L.; Pilski, Jacek
Journal of the Chemical Society, Chemical Communications, 1981 , # 14 p. 703 - 704
反应条件
potassium hydroxide; potassium chloride in isopropyl alcohol
T=25°C; various carbanions and disubstituted diaryl disulfides investigated; Rate constant;
参考文献
Gilbert, H. F.
Journal of the American Chemical Society, 1980 , vol. 102, # 23 p. 7059 - 7065
反应条件
sulfuric acid; nitric acid
T=5 - 10°C;
参考文献
Challenger; Collins
Journal of the Chemical Society, 1924 , vol. 125, p. 1379
Full Text Show Details
Challenger; Higginbottom; Huntington
Journal of the Chemical Society, 1930 , p. 26,29, 31
反应条件
sulfuric acid; nitric acid
T=5 - 10°C;
参考文献
Challenger; Collins
Journal of the Chemical Society, 1924 , vol. 125, p. 1379
Full Text Show Details
Challenger; Higginbottom; Huntington
Journal of the Chemical Society, 1930 , p. 26,29, 31
参考文献
Mueller,H. A.
Chem. Zentralbl., 1906 , vol. 77, # II p. 1588