2,3,4,5,6-五氯氯苄合成路线 (共 10 条)
反应条件
chlorine; KSK silica gel; magnesium chloride T=295 - 320°C; 0.005 h; other methal oxide and chloride catalysts;
参考文献
Potapov; Valitov; Evdokimova
Journal of applied chemistry of the USSR, 1984 , vol. 57, # 2 pt 2 p. 321 - 324
反应条件
phosphorus pentachloride; iodine T=150 - 160°C; im Rohr;
参考文献
Ganguly
Chemische Berichte, 1925 , vol. 58, p. 710
反应条件
hydrogenchloride; acetic acid Electrolysis.im Dunkeln;
参考文献
Beilstein; Kuhlberg
Justus Liebigs Annalen der Chemie, 1869 , vol. 150, p. 294
Justus Liebigs Annalen der Chemie, 1869 , vol. 152, p. 224
参考文献
Kolsaker, Per; Storflor, Harry; Brobakke, Kristin; Carlberg, Georg E.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 9 p. 823 - 832
反应条件
iodine durch Chlorieren; Isolierung des Reaktionsproduktes und erneutes Chlorieren unter Zusatz von SbCl3;
参考文献
Beilstein; Kuhlberg
Justus Liebigs Annalen der Chemie, 1869 , vol. 150, p. 294
Justus Liebigs Annalen der Chemie, 1869 , vol. 152, p. 224
反应条件
aluminum oxide; chlorine; copper dichloride; aluminum oxide; molybdenum(VI) oxide T=300°C; other catalysts, different molar ratio; Product distribution;
参考文献
Potapov; Valitov; Evdokimova
Journal of applied chemistry of the USSR, 1984 , vol. 57, # 2 pt 2 p. 321 - 324
参考文献
Ballester; Molinet
Anales de la Real Sociedad Espanola de Fisica y Quimica, 1958 , vol. <B> 54, p. 151,155
反应条件
T=150 - 160°C; im Rohr;
参考文献
Ganguly
Chemische Berichte, 1925 , vol. 58, p. 710
反应条件
1: sulfuric acid (conc.) / 18 h / 100 °C 2: benzene View Scheme
参考文献
Kolsaker, Per; Storflor, Harry; Brobakke, Kristin; Carlberg, Georg E.
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, 1983 , vol. 37, # 9 p. 823 - 832
反应条件
sulfuric acid
T=100°C; 18 h; Yield given;
参考文献
Hooker Chemicals and Plastics Corporation
Patent: US4075238 A1, 1978 ;