N-(2-亚硝基苯基)-乙酰胺合成路线 （共 7 条）
反应条件
1: With hydrazine; Rh on carbon in tetrahydrofuran T=0°C; 3 h; 2: With tert-butylhypochlorite in tetrahydrofuran T=-78°C; 1 h;
参考文献
Tie, Chenyang; Gallucci, Judith C.; Parquette, Jon R.
Journal of the American Chemical Society, 2006 , vol. 128, # 4 p. 1162 - 1171
反应条件
1.1: AcOH / 4 h / Heating 2.1: hydrazine / Rh/C / tetrahydrofuran / 3 h / 0 °C 2.2: 4.97 g / t-butyl hypochlorite / tetrahydrofuran / 1 h / -78 °C View Scheme
参考文献
Tie, Chenyang; Gallucci, Judith C.; Parquette, Jon R.
Journal of the American Chemical Society, 2006 , vol. 128, # 4 p. 1162 - 1171
反应条件
1: With acetic acid T=100°C; 3 h; 2: With ammonium chloride; zinc in V methoxymethyl ester; water 1.5 h;
参考文献
Reuter, Raphael; Hostettler, Nik; Neuburger, Markus; Wegner, Hermann A.
European Journal of Organic Chemistry, 2009 , # 32 p. 5647 - 5652
反应条件
Potassium peroxomonosulfate in dichloromethane; water T=20°C; 1 h;
参考文献
Bellotto, Silvia; Reuter, Raphael; Heinis, Christian; Wegner, Hermann A.
Journal of Organic Chemistry, 2011 , vol. 76, # 23 p. 9826 - 9834
反应条件
1: ethyl acetate / 0.33 h / 5 °C / Cooling with ice 2: Potassium peroxomonosulfate / dichloromethane; water / 1 h / 20 °C View Scheme
参考文献
Bellotto, Silvia; Reuter, Raphael; Heinis, Christian; Wegner, Hermann A.
Journal of Organic Chemistry, 2011 , vol. 76, # 23 p. 9826 - 9834
参考文献
Green; Rowe
Journal of the Chemical Society, 1917 , vol. 111, p. 618
反应条件
1: azobenzene-2,2'-diamine in toluene
0.25 h; Inert atmosphere;
2: 2-nitrosoacetanilide in toluene
T=60°C; 72 h; Inert atmosphere;
参考文献
Reuter, Raphael; Hostettler, Nik; Neuburger, Markus; Wegner, Hermann A.
European Journal of Organic Chemistry, 2009 , # 32 p. 5647 - 5652
