2,3,5-三甲基-6-(3-甲基丁-2-烯基)环己-2,5-二烯-1,4-二酮合成路线 (共 11 条)
反应条件
mesoporous silica containing bimetallic Cu-Al (CuAl-KIT-5) in 1,2-dichloro-ethane T=60°C; 6 h;
参考文献
Varghese, Shaji; Anand, Chokkalingam; Dhawale, Dattatray; Mane, Gurudas P.; Wahab, Mohammad A.; Mano, Ajayan; Raj, George Allen Gnana; Nagarajan, Samuthira; Vinu, Ajayan
ChemCatChem, 2013 , vol. 5, # 4 p. 899 - 902
反应条件
mesoporous silica containing bimetallic Cu-Al (CuAl-KIT-5) in 1,2-dichloro-ethane T=60°C; 8 h;
参考文献
Varghese, Shaji; Anand, Chokkalingam; Dhawale, Dattatray; Mane, Gurudas P.; Wahab, Mohammad A.; Mano, Ajayan; Raj, George Allen Gnana; Nagarajan, Samuthira; Vinu, Ajayan
ChemCatChem, 2013 , vol. 5, # 4 p. 899 - 902
反应条件
silver(l) oxide in diethyl ether
参考文献
Naruta, Yoshinori
Journal of the American Chemical Society, 1980 , vol. 102, # 11 p. 3774 - 3783
反应条件
tri-n-butyltin methoxide; palladium 1.) dichloroethane, reflux; Yield given. Multistep reaction;
参考文献
Liebeskind, Lanny S.; Foster, Bruce S.
Journal of the American Chemical Society, 1990 , vol. 112, # 23 p. 8612 - 8613
反应条件
1: BF3*OEt2 / CH2Cl2 / -78 °C 2: 142 mg / Ag2O / diethyl ether View Scheme
参考文献
Naruta, Yoshinori
Journal of the American Chemical Society, 1980 , vol. 102, # 11 p. 3774 - 3783
反应条件
1: BF3*OEt2 / CH2Cl2 / -78 °C 2: 142 mg / Ag2O / diethyl ether View Scheme
参考文献
Naruta, Yoshinori
Journal of the American Chemical Society, 1980 , vol. 102, # 11 p. 3774 - 3783
反应条件
CuAl-SBA-15 in cyclohexane T=85°C; 16 h;
参考文献
Varghese, Shaji; Anand, Chokkalinkam; Dhawale, Dattatray; Mano, Ajayan; Balasubramanian, Veerappan V.; Raj, George Allen Gnana; Nagarajan, Samuthira; Wahab, Mohammad A.; Vinu, Ajayan
Tetrahedron Letters, 2012 , vol. 53, # 42 p. 5656 - 5659
反应条件
potassium hydroxide; air; aluminosilicate ASHNTS-3 1) octane, reflux, 2) H2O-CH3OH; Yield given. Multistep reaction;
参考文献
Byzova, V. N.; Zakharova, E. I.; Zhukova, E. E.; Sarycheva, I. K.; Evstigneeva, R. P.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 11 p. 2135 - 2140
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 11 p. 2368 - 2374
反应条件
zeolite HSZ-360 1.) PhCl, 80 deg C, 6 h; Yield given. Multistep reaction;
参考文献
Bigi, Franca; Carloni, Silvia; Maggi, Raimondo; Muchetti, Chiara; Rastelli, Massimo; Sartori, Giovanni
Synthesis, 1998 , # 3 p. 301 - 304
反应条件
1: (i) NaOCH2CH2OMe, (ii) /BRN= 505943/ 2: (i) Ni(CO)4, (ii) /BRN= 7116912/, (iii) aq. FeCl3 View Scheme
参考文献
Sato; Inoue; Yamaguchi
The Journal of organic chemistry, 1972 , vol. 37, # 12 p. 1889 - 1892