Boc-O-苄基-L-酪氨酸合成路线 （共 34 条）
反应条件
sodium methylate; tetra-(n-butyl)ammonium iodide in methanol T=40°C; 3 h;
参考文献
AJINOMOTO, CO., INC.
Patent: US2005/283021 A1, 2005 ;
Location in patent: Page/Page column 6 ;
反应条件
1: With sodium methylate; tetra-(n-butyl)ammonium iodide in methanol T=40°C; 24 h; 2: With hydrogenchloride in methanol; water
参考文献
AJINOMOTO, CO., INC.
Patent: US2005/283021 A1, 2005 ;
Location in patent: Page/Page column 6 ;
反应条件
1: [125I]-L-Tyrosine With sodium hydroxide in water 1.5 h; 2: With copper(II) sulfate in water 0.5 h; 3: di-tert-butyl dicarbonate; benzyl bromide
参考文献
Shanghai Institute Of Materia Medica Chinese Academy of Sciences
Patent: EP2133342 A1, 2009 ;
Location in patent: Page/Page column 32 ;
反应条件
triethylamine; citric acid in 1,4-dioxane; water
参考文献
US6083903 A1, ;
US5780454 A1, ;
US 5780454 A
反应条件
in water; tert-butyl alcohol pH 9.5-10.0;
参考文献
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 40, # 4 p. 235 - 241
Acta Chemica Scandinavica, Series B: Organic Chemistry and Biochemistry, , vol. 40, # 4 p. 250 - 256
参考文献
Monatshefte fuer Chemie, , vol. 105, p. 1110 - 1135
反应条件
1.1: aq. NaOH; CuSO4*5H2O / 1 h / Heating 1.2: 73 percent / aq. NaOH / methanol / 20 °C 2.1: aq. NaOH; NaHCO3 / dioxane / 20 °C View Scheme
参考文献
Croatica Chemica Acta, , vol. 76, # 1 p. 23 - 36
反应条件
1.1: aq. NaOH; CuSO4*5H2O / 1 h / Heating 1.2: 73 percent / aq. NaOH / methanol / 20 °C 2.1: aq. NaOH; NaHCO3 / dioxane / 20 °C View Scheme
参考文献
Croatica Chemica Acta, , vol. 76, # 1 p. 23 - 36
反应条件
triethylamine in tert-butyl alcohol
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 2632 - 2636
反应条件
1,4-dioxane; sodium hydroxide anschliessendes Erwaermen mit Azidokohlensaeure-tert-butylester;
参考文献
Helvetica Chimica Acta, , vol. 42, p. 2622
