N-异丙基-4-甲基苯磺酰胺合成路线 （共 20 条）
反应条件
trifluorormethanesulfonic acid in toluene T=120°C; 14 h;
参考文献
Shi, Wei; Bai, Chun-Mei; Zhu, Kai; Cui, Dong-Mei; Zhang, Chen
Tetrahedron, 2014 , vol. 70, # 2 p. 434 - 438
反应条件
perchloric acid adsorbed on silica gel in 1,4-dioxane T=80°C; 3 h;
参考文献
Das, Biswanath; Reddy, Parigi Raghavendar; Sudhakar, Chithaluri; Lingaiah, Maram
Tetrahedron Letters, 2011 , vol. 52, # 27 p. 3521 - 3522
反应条件
triethylamine; 1-(toluene-p-sulphonyl)imidazole in N,N-dimethyl-formamide Reflux;
参考文献
Rad, Mohammad Navid Soltani; Behrouz, Somayeh; Nekoei, Abdo-Reza
Phosphorus, Sulfur and Silicon and the Related Elements, 2014 , vol. 189, # 4 p. 465 - 476
反应条件
sodium tetrahydroborate; Hg(NO3)2; N-butylamine 1.) methylene dichloride, reflux, 8 h, 2.) aq. sodium hydroxide; Yield given. Multistep reaction;
参考文献
Karshtedt, Dmitry; Bell, Alexis T.; Tilley, T. Don
Journal of the American Chemical Society, 2005 , vol. 127, # 36 p. 12640 - 12646
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine in dichloromethane T=0 - 20°C; 16 h;
参考文献
Clavier, Herve; Lepronier, Aymeric; Bengobesse-Mintsa, Nathalie; Gatineau, David; Pellissier, Helene; Giordano, Laurent; Tenaglia, Alphonse; Buono, Gerard
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 2-3 p. 403 - 408
反应条件
tetraethylammonium p-toluenesulfonate in methanol Electrochemical reactionreticulated vitreous carbon anode; Pt cathode;
参考文献
D'Oca, Marcelo G. Montes; Russowsky, Dennis; Canto, Karen; Gressler, Tanara; Goncalves, Reinaldo S.
Organic Letters, 2002 , vol. 4, # 10 p. 1763 - 1766
反应条件
1: With 2,4,6-trichloro-1,3,5-triazine in acetonitrile T=20°C; 0.5 h; 2: With triethylamine in acetonitrile
参考文献
Rad, Mohammad Navid Soltani; Khalafi-Nezhad, Ali; Asrari, Zeinab; Behrouz, Somayeh; Amini, Zohreh; Behrouz, Marzieh
Synthesis, 2009 , # 23 art. no. Z15009SS, p. 3983 - 3988
反应条件
1: n-butyllithium / tetrahydrofuran 2: 81 percent / tetraethylammonium p-toluenesulfonate / methanol / Electrochemical reaction; reticulated vitreous carbon anode; Pt cathode View Scheme
参考文献
D'Oca, Marcelo G. Montes; Russowsky, Dennis; Canto, Karen; Gressler, Tanara; Goncalves, Reinaldo S.
Organic Letters, 2002 , vol. 4, # 10 p. 1763 - 1766
反应条件
1: 85 percent / thionyl chloride 2: n-butyllithium / tetrahydrofuran 3: 81 percent / tetraethylammonium p-toluenesulfonate / methanol / Electrochemical reaction; reticulated vitreous carbon anode; Pt cathode View Scheme
参考文献
D'Oca, Marcelo G. Montes; Russowsky, Dennis; Canto, Karen; Gressler, Tanara; Goncalves, Reinaldo S.
Organic Letters, 2002 , vol. 4, # 10 p. 1763 - 1766
参考文献
Monjoint, Pierre; Ruasse, Marie-Francoise
Tetrahedron Letters, 1984 , vol. 25, # 30 p. 3183 - 3186
