苯甲醇-Alpha,Alpha-d2合成路线 (共 34 条)
反应条件
1: 1) SOCl2, 2) Mg 2: LiAlD4 View Scheme
参考文献
Gessner, Uwe; Heesing, Albert
Chemische Berichte, 1985 , vol. 118, # 7 p. 2593 - 2606
反应条件
3 A molecular sieve; pyridinium chlorochromate in dichloromethane T=25°C; 4 h;
参考文献
O'Hagan, David; Goss, Rebecca J. M.; Meddour, Abdelkrim; Courtieu, Jacques
Journal of the American Chemical Society, 2003 , vol. 125, # 2 p. 379 - 387
反应条件
[{(η5-C5Me5)IrCl}2(μ-Cl)2]; oxygen; triethylamine in toluene T=80°C; P=760.051 Torr; Kinetics;
参考文献
Jiang, Bi; Feng, Yuee; Ison, Elon A.
Journal of the American Chemical Society, 2008 , vol. 130, # 44 p. 14462 - 14464
反应条件
lithium perchlorate in acetonitrile competitive anodic oxidation; isotope effect; Product distribution;
参考文献
Boyd, Jean W.; Schmalzl, Paul W.; Miller, Larry L.
Journal of the American Chemical Society, 1980 , vol. 102, # 11 p. 3856 - 3862
反应条件
water; palladium diacetate; diphenylphosphinobenzene-3-sulfonic acid sodium salt T=120°C; 16 h; Sealed tube;
参考文献
Hikawa, Hidemasa; Matsuda, Naoya; Suzuki, Hideharu; Yokoyama, Yuusaku; Azumaya, Isao
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 11-12 p. 2308 - 2320
反应条件
in dichloromethane T=19.84°C; Kinetics;
参考文献
Asami, Kazutaka; Tsukidate, Kazuaki; Iwatsuki, Satoshi; Tani, Fumito; Karasawa, Satoru; Chiang, Linus; Storr, Tim; Thomas, Fabrice; Shimazaki, Yuichi
Inorganic Chemistry, 2012 , vol. 51, # 22 p. 12450 - 12461
反应条件
pyridine; thionyl chloride in dichloromethane T=20°C; 12 h;
参考文献
Biellmann, Jean-Francois; d'Orchymont, Hugues
Journal of Organic Chemistry, 1982 , vol. 47, # 15 p. 2882 - 2886
反应条件
1: 63 percent / PCC / CH2Cl2 / 3 h / 0 - 20 °C 2: 45 percent / trichloroacetic acid / dimethylformamide / 3 h / 20 °C 3: 2 percent Chromat. / CrCl2 / tetrahydrofuran; H2O / 3 h / 20 °C View Scheme
参考文献
Bejot, Romain; Tisserand, Steve; Li, De Run; Falck; Mioskowski, Charles
Tetrahedron Letters, 2007 , vol. 48, # 22 p. 3855 - 3858
反应条件
palladium diacetate; diphenylphosphinobenzene-3-sulfonic acid sodium salt in water-d2 T=120°C; 16 h; sealed tubeInert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 77, # 16 p. 7046 - 7051
反应条件
palladium diacetate; diphenylphosphinobenzene-3-sulfonic acid sodium salt in water T=120°C; 16 h; sealed tubeInert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 77, # 16 p. 7046 - 7051