三乙氧基(4-甲氧苯基)硅烷合成路线 （共 36 条）
反应条件
Pd((CH3)2C6H3NC(CH3)CHC(CH3)NC6H3(CH3)2)(CH3)(P(CH2CH3)3); tetrabutylammomium bromide; sodium hydroxide in water T=80°C; Hiyama coupling; 10 h; Inert atmosphere;
参考文献
Lee, Dong-Hwan; Jung, Ji-Young; Jin, Myung-Jong
Chemical Communications, 2010 , vol. 46, # 47 p. 9046 - 9048
反应条件
NH4I; potassium fluoride; Cu(NO3)2*3H2O; oxygen T=140°C; 25 h; Schlenk technique; Reagent/catalystSolventTemperature;
参考文献
Wang, Zhen; Chang, Sukbok
Organic Letters, 2013 , vol. 15, # 8 p. 1990 - 1993
反应条件
1: Cu(NO3)2*3H2O; potassium fluoride; oxygen; NH4I / N,N-dimethyl-formamide / 0.5 h / 140 °C / |Schlenk technique 2: Cu(NO3)2*3H2O; oxygen; NH4I / 25 h / 140 °C / |Schlenk technique View Scheme
参考文献
Wang, Zhen; Chang, Sukbok
Organic Letters, 2013 , vol. 15, # 8 p. 1990 - 1993
反应条件
sodium hydroxide; methyl-ethyl phosphite; dichloro bis(acetonitrile) palladium(II) in 1,4-dioxane T=80°C; 8 h;
参考文献
Murata; Shimazaki; Watanabe; Masuda
Synthesis, 2001 , # 15 p. 2231 - 2233
反应条件
silver fluoride in N,N-dimethyl-formamide T=80°C; 24 h;
参考文献
Luo, Hai-Qing; Dong, Wen
Synthetic Communications, 2013 , vol. 43, # 20 p. 2733 - 2738
反应条件
potassium carbonate in tetrahydrofuran
T=70°C; 10 h;
参考文献
Bhadra, Sukalyan; Saha, Amit; Ranu, Brindaban C.
Journal of Organic Chemistry, 2010 , vol. 75, # 14 p. 4864 - 4867
反应条件
3-benzyl-1-(2-hydroxy-2-phenylethyl)imidazolium chloride; tetrabutylammomium bromide; water; palladium diacetate; sodium hydroxide
T=120°C; Hiyama coupling; 1 h; Microwave irradiation;
参考文献
Penafiel, Itziar; Pastor, Isidro M.; Yus, Miguel; Esteruelas, Miguel A.; Olivan, Montserrat; Onate, Enrique
European Journal of Organic Chemistry, 2011 , # 35 p. 7174 - 7181
反应条件
tetrabutyl ammonium fluoride; palladium in tetrahydrofuran
T=70°C; Hiyama coupling; 2 h; Inert atmosphere;
参考文献
Srimani, Dipankar; Bej, Ansuman; Sarkar, Amitabha
Journal of Organic Chemistry, 2010 , vol. 75, # 12 p. 4296 - 4299
反应条件
[2,2']bipyridinyl; CuF2; [(diglyme)NiBr2]; cesium fluoride in N,N-dimethyl acetamide
T=150°C; 2.5 h; Inert atmosphere;
参考文献
Hachiya, Hitoshi; Hirano, Koji; Satoh, Tetsuya; Miura, Masahiro
Angewandte Chemie - International Edition, 2010 , vol. 49, # 12 p. 2202 - 2205
反应条件
3-benzyl-1-(2-hydroxy-2-phenylethyl)imidazolium chloride; water; palladium diacetate; sodium hydroxide
T=120°C; Hiyama coupling; 1 h; Microwave irradiation;
参考文献
Penafiel, Itziar; Pastor, Isidro M.; Yus, Miguel; Esteruelas, Miguel A.; Olivan, Montserrat; Onate, Enrique
European Journal of Organic Chemistry, 2011 , # 35 p. 7174 - 7181
