4,5-二甲氧基-1,2-苯并醌合成路线 （共 46 条）
反应条件
lead(IV) acetate in acetic acid
T=80°C; 12 h;
参考文献
Cole, Edward R.; Crank, George; Minh, H. T. Hai
Australian Journal of Chemistry, 1980 , vol. 33, # 3 p. 527 - 543
反应条件
Fremy’s salt in water
Na2HPO4-NaH2PO4 buffer pH=5.8;
参考文献
Deya, Pedro M.; Dopico, Mercedes; Raso, Angel Garcia; Morey, Jeronimo; Saa, Jose M.
Tetrahedron, 1987 , vol. 43, # 15 p. 3523 - 3532
反应条件
1: sodium borohydride / tetrahydrofuran
2: 85 percent / (KSO3)2NO / H2O / Na2HPO4-NaH2PO4 buffer pH=5.8
View Scheme
参考文献
Deya, Pedro M.; Dopico, Mercedes; Raso, Angel Garcia; Morey, Jeronimo; Saa, Jose M.
Tetrahedron, 1987 , vol. 43, # 15 p. 3523 - 3532
反应条件
1: Cu2Cl2, Cu, O2 / acetonitrile / 4 h / 25 °C
2: DBU / acetonitrile; various solvent(s) / 1.5 h / 0 °C
View Scheme
参考文献
Reinaud, Olivia; Capdevielle, Patrice; Maumy, Michel
Tetrahedron Letters, 1985 , vol. 26, # 33 p. 3993 - 3996
反应条件
[Cu(phenanthroline)2]chlorite
40 h;
参考文献
Hossain, Md. Munkir; Tseng, Mei-Chun; Lee, Chi-Rung; Shyu, Shin-Guang
European Journal of Inorganic Chemistry, 2014 , # 1 p. 36 - 40
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene in acetonitrile
-30 deg C, 1 h; -20 deg C, 5 h;
参考文献
Reinaud, Olivia; Capdevielle, Patrice; Maumy, Michel
Synthesis, 1988 , # 4 p. 293 - 300
反应条件
lead(IV) acetate
T=16°C; 0.5 h;
参考文献
Cole, Edward R.; Crank, George; Minh, H. T. Hai
Australian Journal of Chemistry, 1980 , vol. 33, # 3 p. 527 - 543
反应条件
lead(IV) acetate
T=20°C; 1 h;
参考文献
Cole, Edward R.; Crank, George; Minh, H. T. Hai
Australian Journal of Chemistry, 1980 , vol. 33, # 3 p. 527 - 543
反应条件
1: 73 percent / LiAlH4 / diethyl ether / 2 h / Heating
2: 75 percent / 40percent sodium hydroxide / acetone / 1 h
3: 180 mg / lead tetraacetate / 1 h / 20 °C
View Scheme
参考文献
Cole, Edward R.; Crank, George; Minh, H. T. Hai
Australian Journal of Chemistry, 1980 , vol. 33, # 3 p. 527 - 543
反应条件
1: 75 percent / 40percent sodium hydroxide / acetone / 1 h
2: 180 mg / lead tetraacetate / 1 h / 20 °C
View Scheme
参考文献
Cole, Edward R.; Crank, George; Minh, H. T. Hai
Australian Journal of Chemistry, 1980 , vol. 33, # 3 p. 527 - 543
