乙酰溴-Alpha-D-葡萄糖酮酸甲基酯合成路线 （共 53 条）
参考文献
Engstrom, Kenneth M.; Henry, Rodger F.; Marsden, Ian
Tetrahedron Letters, 2007 , vol. 48, # 8 p. 1359 - 1362
反应条件
quinoline; silver(l) oxide
参考文献
Lunsford; Murphey
Journal of Organic Chemistry, 1956 , vol. 21, p. 580,582
反应条件
1: 3.4 percent / K2CO3 / acetone / 6 h / Heating 2: 59.2 percent / 0.2 N aq. NaOH / acetone / 2 h / Ambient temperature View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 40, # 1 p. 131 - 135
反应条件
anhydrous cadmium carbonate in water; acetonitrile T=70°C; 4 h;
参考文献
Casati, Silvana; Ottria, Roberta; Ciuffreda, Pierangela
Steroids, 2009 , vol. 74, # 2 p. 250 - 255
反应条件
1: 72 percent / Ag2CO3 / benzene / 48 h / Ambient temperature 2: 83 percent / NaBH4, PdCl2 / methanol / 2 h / 0 °C 3: 44 percent / aq. 2M NaOH / methanol / Ambient temperature View Scheme
参考文献
Numazawa, Mitsuteru; Nagaoka, Masao; Tsuji, Masachika; Osawa, Yoshio
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 1 p. 121 - 125
反应条件
1: 73 percent / Ag2O 2: H2 / Pd/C View Scheme
参考文献
Engstrom, Kenneth M.; Henry, Rodger F.; Marsden, Ian
Tetrahedron Letters, 2007 , vol. 48, # 8 p. 1359 - 1362
反应条件
silver(l) oxide Multistep reaction. Further byproducts given;
参考文献
Dawson, Marcia I.; Hobbs, Peter D.
Carbohydrate Research, 1980 , vol. 85, p. 121 - 129
反应条件
isoquinoline; silver(l) oxide T=20°C; 1 h;
参考文献
Rossignol, Jean-Francois; Stachulski, Andrew V.
Journal of Chemical Research - Part S, 1999 , # 1 p. 44 - 45
反应条件
1: 61 percent / Ag2O, isoquinoline / 1 h / 20 °C 2: 80 percent / cyclohexene / Pd/C / propan-2-ol / 0.5 h / Heating 3: 67 percent / 1-(3-dimethylaminopropyl)-3-ethylcarbodiimide hydrochloride, 4-N,N-dimethylaminopyridine, 1-hydroxybenzotriazole monohydrate / dimethylformamide / a) 20 deg C, 2 h, b) 0 deg C, 16 h View Scheme
参考文献
Journal of Chemical Research - Part S, , # 1 p. 44 - 45
反应条件
1.1: Ag2O; CaSO4; pyridine / AcOH 1.2: cyclohexene / Pd(OH)2/C / ethanol / 0.5 h / Heating 2.1: 89 mg / Na2CO3 / aq. methanol / 2.5 h / 20 °C View Scheme
参考文献
Needs, Paul W.; Kroon, Paul A.
Tetrahedron, 2006 , vol. 62, # 29 p. 6862 - 6868
