5,6-二甲氧基-1-茚酮合成路线 （共 60 条）
反应条件
pyridine; palladium diacetate; tetrabutyl-ammonium chloride in N,N-dimethyl-formamide T=100°C; P=760 Torr; 24 h;
参考文献
Gagnier, Steve V.; Larock, Richard C.
Journal of the American Chemical Society, 2003 , vol. 125, # 16 p. 4804 - 4807
反应条件
methanesulfonic acid; phosphorus pentoxide T=100°C; 0.05 h;
参考文献
Cho, Hidetsura; Matsuki, Shinsuke
Heterocycles, 1996 , vol. 43, # 1 p. 127 - 131
反应条件
pyridine; tetrabutyl-ammonium chloride; [(t-Bu)3PH]BF4; palladium diacetate in N,N-dimethyl-formamide T=130°C; 0.333333 h; microwave irradiation;
参考文献
Wu, Xiongyu; Nilsson, Peter; Larhed, Mats
Journal of Organic Chemistry, 2005 , vol. 70, # 1 p. 346 - 349
反应条件
[rhenium(pentacarbonyl)(bromide)] in 1,2-dichloro-ethane 2 h; Heating;
参考文献
Kusama, Hiroyuki; Narasaka, Koichi
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 8 p. 2379 - 2384
反应条件
scandium tris(trifluoromethanesulfonate) in nitromethane T=100°C; Friedel-Crafts acylation; 0.75 h;
参考文献
Fillion, Eric; Fishlock, Dan; Wilsily, Ashraf; Goll, Julie M.
Journal of Organic Chemistry, 2005 , vol. 70, # 4 p. 1316 - 1327
反应条件
AlCl3, aluminium chloride in dichloromethane T=0 - 20°C; Friedel-Crafts Acylation; Inert atmosphere; regioselective reaction;
参考文献
Chavan, Subhash P.; Garai, Sumanta; Dutta, Achintya Kumar; Pal, Sourav
European Journal of Organic Chemistry, 2012 , # 35 p. 6841 - 6845
反应条件
bis(1,5-cyclooctadiene)-rhodium(I) tetrafluoroborate; 6-diphenylphosphinomethyl-3-methyl-2-aminopyridine in toluene T=150°C; 1 h; Inert atmosphere;
参考文献
Vautravers, Nicolas R.; Regent, Damien D.; Breit, Bernhard
Chemical Communications, 2011 , vol. 47, # 23 p. 6635 - 6637
反应条件
Tb(OTf)3 in chlorobenzene T=250°C; Friedel-Crafts reaction; 1 h;
参考文献
Tetrahedron Letters, , vol. 45, # 8 p. 1741 - 1745
反应条件
1.1: n-BuLi / tetrahydrofuran / 0.5 h / 0 °C 1.2: 90 percent / tetrahydrofuran 2.1: 82 percent / Pd(OAc)2; pyridine; n-Bu4NCl / dimethylformamide / 24 h / 100 °C / 760 Torr View Scheme
参考文献
Journal of the American Chemical Society, , vol. 125, # 16 p. 4804 - 4807
反应条件
trifluoromethanesulfonic acid anhydride in 1,2-dichloro-ethane 6 h; Heating;
参考文献
Nenajdenko, Valentine G.; Baraznenok, Ivan L.; Balenkova, Elizabeth S.
Tetrahedron Letters, 1996 , vol. 37, # 24 p. 4199 - 4202
