1-氯-2,4,6-三氟苯合成路线 （共 13 条）
反应条件
in N,N-dimethyl-formamide
参考文献
SDS Biotech K.K.
Patent: US5510533 A1, 1996 ;
反应条件
copper; zinc in water; N,N-dimethyl-formamide T=70°C; 10 h;
参考文献
Russian Journal of Organic Chemistry, , vol. 36, # 10 p. 1488 - 1499
反应条件
(2,2'-bipyridine-N,N')dichloronickel; zinc in water; N,N-dimethyl-formamide T=80°C; Dehalogenation; 3 h;
参考文献
Trukhin; Adonin; Starichenko
Russian Journal of Organic Chemistry, 2000 , vol. 36, # 1 p. 132 - 133
反应条件
1: iron; aqueous NH4Cl 3: iron; chlorine View Scheme
参考文献
Journal of the American Chemical Society, , vol. 73, p. 153
Journal of the American Chemical Society, , vol. 81, p. 94,98
反应条件
1: sulfuric acid; aqueous phosphoric acid; nitrosylsulfuric acid / anschliessendes Behandeln mit Natriumhypophosphit-Loesung und Kupfer(I)-oxid 2: iron; aqueous NH4Cl 4: iron; chlorine View Scheme
参考文献
Journal of the American Chemical Society, , vol. 73, p. 153
Journal of the American Chemical Society, , vol. 81, p. 94,98
反应条件
2: iron; chlorine View Scheme
参考文献
Journal of the American Chemical Society, , vol. 73, p. 153
Journal of the American Chemical Society, , vol. 81, p. 94,98
反应条件
1: H2SO4; HNO3 2: sulfuric acid; aqueous phosphoric acid; nitrosylsulfuric acid / anschliessendes Behandeln mit Natriumhypophosphit-Loesung und Kupfer(I)-oxid 3: iron; aqueous NH4Cl 5: iron; chlorine View Scheme
参考文献
Journal of the American Chemical Society, , vol. 73, p. 153
Journal of the American Chemical Society, , vol. 81, p. 94,98
参考文献
Journal of the American Chemical Society, , vol. 73, p. 153
Journal of the American Chemical Society, , vol. 81, p. 94,98
反应条件
zinc copper in water; N,N-dimethyl-formamide T=70°C; 10 h; other polyfluoroarenes and polyfluorinated olefins; other temperature and time;
参考文献
Russian Journal of Organic Chemistry, , vol. 30, # 8 p. 1336 - 1340
Zhurnal Organicheskoi Khimii, , vol. 30, # 8 p. 1271 - 1275
反应条件
potassium fluoride; water T=480°C; 19 h; variation of amt. of H2O; Product distribution;
参考文献
Journal of Fluorine Chemistry, , vol. 18, p. 101 - 116
