4-[(E)-6,7-二羟基-3,7-二甲基辛-2-烯氧基]-1H-喹啉-2-酮合成路线 (共 3 条)
反应条件
osmium(VIII) oxide in pyridine; diethyl ether 24 h;
参考文献
Grundon Michael F.; Ramachandran, V. N.; Donnelly, Michael E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 633 - 635
反应条件
1: 3.4 g / K2CO3 / acetone / 240 h / Heating 2: 1.2 g / m-chloroperbenzoic acid / CHCl3 / 120 h / Ambient temperature 3: 1.0 g / 24 h / Ambient temperature 4: 0.8 g / aq. KOH / methanol / 6 h / Ambient temperature View Scheme
参考文献
Grundon Michael F.; Ramachandran, V. N.; Donnelly, Michael E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 633 - 635
反应条件
1: 3.4 g / K2CO3 / acetone / 240 h / Heating 2: 1.2 g / m-chloroperbenzoic acid / CHCl3 / 120 h / Ambient temperature 3: 1.0 g / 24 h / Ambient temperature 4: 0.8 g / aq. KOH / methanol / 6 h / Ambient temperature View Scheme
参考文献
Grundon Michael F.; Ramachandran, V. N.; Donnelly, Michael E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 633 - 635