pyridine; thionyl chloride

lithium chloride

thionyl chloride

chlorine T=-9°C; Irradiation;

暂无反应条件数据

sodium acetate; acetic acid; tetracarbonylnickel(0)

暂无反应条件数据

zinc(II) chloride in dichloromethane 72 h; Ambient temperature;

n-butyllithium in tetrahydrofuran BuLi in hexane was cautiously added under N2 at -100°C to a stirred soln. of propargylic chloride in THF, after 10 min Ph3SnCl was added, mixt. was stirred at -60°C for 0.5 h, allowed to warm to room temp.; mixt. was poured into satd. aq. NH4Cl, extd. with 1:1 ether-pentane, combined exts. were washed with water, dried over MgSO4, evapd. in vacuo;

diisobutylaluminium hydride; triphenylphosphine; palladium dichloride in tetrahydrofuran 1 h; Ambient temperature;