1-苯基-2,8,9-三氧杂-5-氮杂-1-硅杂二环[3.3.3]十一烷合成路线 (共 44 条)
反应条件
tetrabutyl ammonium fluoride; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran 2 h; Heating;
参考文献
Riggleman, Shaundra; DeShong, Philip
Journal of Organic Chemistry, 2003 , vol. 68, # 21 p. 8106 - 8109
反应条件
tetrabutyl ammonium fluoride; 2-dicyclohexylphosphino-1,1'-biphenyl; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran 12 h; Heating;
参考文献
Riggleman, Shaundra; DeShong, Philip
Journal of Organic Chemistry, 2003 , vol. 68, # 21 p. 8106 - 8109
反应条件
in not given warming with NH4F-HF; splitting into water, extraction with ether;
参考文献
Zeitschrift fuer Anorganische und Allgemeine Chemie, , vol. 1969, p. 368 - 368
Bi: Org.Verb., 1.3.3.2.4.1, page 62 - 68
FR1559505 , ;
C.A, , vol. 72, p. 43877
反应条件
tetrabutyl ammonium fluoride; 2-dicyclohexylphosphino-1,1'-biphenyl; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran 12 h; Heating;
参考文献
Riggleman, Shaundra; DeShong, Philip
Journal of Organic Chemistry, 2003 , vol. 68, # 21 p. 8106 - 8109
反应条件
tetrabutyl ammonium fluoride; triphenylphosphine; palladium diacetate in tetrahydrofuran; N,N-dimethyl-formamide T=90°C; 2 h;
参考文献
Riggleman, Shaundra; DeShong, Philip
Journal of Organic Chemistry, 2003 , vol. 68, # 21 p. 8106 - 8109
反应条件
tetrabutyl ammonium fluoride; triphenylphosphine; palladium diacetate in tetrahydrofuran; N,N-dimethyl-formamide Heating;
参考文献
Riggleman, Shaundra; DeShong, Philip
Journal of Organic Chemistry, 2003 , vol. 68, # 21 p. 8106 - 8109
反应条件
tetrabutyl ammonium fluoride; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran 2 h; Heating;
参考文献
Riggleman, Shaundra; DeShong, Philip
Journal of Organic Chemistry, 2003 , vol. 68, # 21 p. 8106 - 8109
反应条件
tetrabutyl ammonium fluoride; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in tetrahydrofuran 2 h; Heating;
参考文献
Riggleman, Shaundra; DeShong, Philip
Journal of Organic Chemistry, 2003 , vol. 68, # 21 p. 8106 - 8109
反应条件
in hexadeuterioacetone Kinetics; byproducts: ClSi(OCH2CH2)3N; not isolated, reaction followed by (1)H-NMR spectroscopy;
参考文献
Nies, J. Dirk; Bellama, Jon M.; Ben-Zvi, Nava
Journal of Organometallic Chemistry, 1985 , vol. 296, p. 315 - 320
反应条件
3-benzyl-1-(2-hydroxy-2-phenylethyl)imidazolium chloride; water; palladium diacetate; sodium hydroxide T=120°C; Hiyama coupling; 1 h; Microwave irradiation;
参考文献
Penafiel, Itziar; Pastor, Isidro M.; Yus, Miguel; Esteruelas, Miguel A.; Olivan, Montserrat; Onate, Enrique
European Journal of Organic Chemistry, 2011 , # 35 p. 7174 - 7181