6-溴苯并二氢吡喃-2-酮合成路线 （共 14 条）
反应条件
4-(N,N-dimethlyamino)pyridine; 4-mesityl-3-(4-methoxyphenyl)-1-phenyl-4H-1,2,4-triazol-1-ium perchlorate in ethyl acetate T=80°C; 15 h; Inert atmosphere;
参考文献
Zeitler, Kirsten; Rose, Christopher A.
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1759 - 1762
反应条件
aluminium trichloride; nitrobenzene
参考文献
Barnes; Kraft; Gordon
Journal of the American Chemical Society, 1949 , vol. 71, p. 3523,3527
反应条件
1: tetrachloromethane; bromine / -10 °C 2: aluminium chloride; benzene View Scheme
参考文献
Barnes; Kraft; Gordon
Journal of the American Chemical Society, 1949 , vol. 71, p. 3523,3527
反应条件
1: ethanol / 180 °C / Erhitzen des Reaktionsprodukts mit wss.-methanol. Kalilauge 2: aluminium chloride; benzene View Scheme
参考文献
Barnes; Kraft; Gordon
Journal of the American Chemical Society, 1949 , vol. 71, p. 3523,3527
反应条件
glucose-6-phosphate dehydrogenase; glucose-6-phosphate; 4-hydroxyacetophenone monooxygenase; NADPH T=20°C; Baeyer-Villiger oxidation; pH=9; 72 h; aq. Tris-HCl bufferEnzymatic reaction;
参考文献
Rioz-Martinez, Ana; De Gonzalo; Torres Pazmino, Daniel E.; Fraaije, Marco W.; Gotor, Vicente
European Journal of Organic Chemistry, 2009 , # 15 p. 2526 - 2532
反应条件
1: carbon disulfide; bromine / im Sonnenlicht View Scheme
参考文献
Fittig; Hochstetter
Justus Liebigs Annalen der Chemie, 1884 , vol. 226, p. 359
反应条件
1: diluted alcohol; sodium amalgam / 40 - 60 °C View Scheme
参考文献
Lasch
Monatshefte fuer Chemie, 1913 , vol. 34, p. 1660
参考文献
Lasch
Monatshefte fuer Chemie, 1913 , vol. 34, p. 1660
反应条件
1: titanocene bis(p-chlorophenoxide), polymethylhydrosiloxane / tetrahydrofuran / Ambient temperature 2: Et3SiH, Amberlyst 15 / CH2Cl2 / Ambient temperature View Scheme
参考文献
Hansen, Marcus C.; Verdaguer, Xavier; Buchwald, Stephen L.
Journal of Organic Chemistry, 1998 , vol. 63, # 7 p. 2360 - 2361
反应条件
lithium aluminium tetrahydride in diethyl ether
参考文献
Billman; Tonnis
Journal of pharmaceutical sciences, 1971 , vol. 60, # 8 p. 1188 - 1192
