1,2-Dithiaacenaphthene合成路线 （共 4 条）
反应条件
sodium tetrahydroborate in tetrahydrofuran; ethanol T=5°C; 1 h; Inert atmosphere;
参考文献
Grainger, Richard S.; Patel, Bhaven; Kariuki, Benson M.; Male, Louise; Spencer, Neil
Journal of the American Chemical Society, 2011 , vol. 133, # 15 p. 5843 - 5852
反应条件
1: With trichlorophosphate
T=0 - 20°C; Vilsmeier formylation;
2: With water
Further stages.;
参考文献
Miller, Evan W.; Bian, Shelly X.; Chang, Christopher J.
Journal of the American Chemical Society, 2007 , vol. 129, # 12 p. 3458 - 3459
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane
T=0 - 20°C; 2.5 h; Inert atmosphere;
参考文献
Grainger, Richard S.; Patel, Bhaven; Kariuki, Benson M.
Angewandte Chemie, International Edition, 2009 , vol. 48, p. 4832 - 4835
Angewandte Chemie, 2009 , vol. 121, p. 4926 - 4929
反应条件
titanium(III) chloride; dihydrogen peroxide in methanol; water
0.0833333 h; Ambient temperature;
参考文献
Oae, Shigeru; Nabeshima, Tatsuya; Takata, Toshikazu
Heterocycles, 1982 , vol. 18, p. 41 - 44
