6-甲基-3(2H)-苯并呋喃酮合成路线 (共 8 条)
反应条件
1: 70 percent / xylene / 40 h / Heating 2: 82 percent / KOH / ethanol; H2O View Scheme
参考文献
Deshpande, A. R.; Paradkar, M. V.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 8 p. 526 - 528
反应条件
potassium fluoride in N,N-dimethyl-formamide
0.25 h; Ambient temperature;
参考文献
Gonzalez, Antonio G.; Barrera, Jaime Bermejo; Hernandez, Carlos Yanes
Heterocycles, 1992 , vol. 34, # 7 p. 1311 - 1315
反应条件
sodium acetate; copper(ll) bromide in ethanol; ethyl acetate
参考文献
NEUROSCIENZE PHARMANESS S.C. A.R.L.
Patent: US2010/215741 A1, 2010 ;
反应条件
1: 75 percent / pyridine / Ambient temperature
2: 43.9 percent / Br2 / CHCl3 / 0.33 h / Heating
3: 40.4 percent / KF / dimethylformamide / 0.25 h / Ambient temperature
View Scheme
参考文献
Gonzalez, Antonio G.; Barrera, Jaime Bermejo; Hernandez, Carlos Yanes
Heterocycles, 1992 , vol. 34, # 7 p. 1311 - 1315
反应条件
1: 90.5 percent / AlCl3 / CS2 / 4 h / 140 °C
2: 75 percent / pyridine / Ambient temperature
3: 43.9 percent / Br2 / CHCl3 / 0.33 h / Heating
4: 40.4 percent / KF / dimethylformamide / 0.25 h / Ambient temperature
View Scheme
参考文献
Gonzalez, Antonio G.; Barrera, Jaime Bermejo; Hernandez, Carlos Yanes
Heterocycles, 1992 , vol. 34, # 7 p. 1311 - 1315
反应条件
1: 43.9 percent / Br2 / CHCl3 / 0.33 h / Heating
2: 40.4 percent / KF / dimethylformamide / 0.25 h / Ambient temperature
View Scheme
参考文献
Gonzalez, Antonio G.; Barrera, Jaime Bermejo; Hernandez, Carlos Yanes
Heterocycles, 1992 , vol. 34, # 7 p. 1311 - 1315
反应条件
1: thionyl chloride
2: aluminium chloride; carbon disulfide
View Scheme
参考文献
Mameli
Gazzetta Chimica Italiana, 1926 , vol. 56, p. 764
Full Text Show Details
Higginbotham; Stephen
Journal of the Chemical Society, 1920 , vol. 117, p. 1541
反应条件
1: alkali
2: thionyl chloride
3: aluminium chloride; carbon disulfide
View Scheme
参考文献
Mameli
Gazzetta Chimica Italiana, 1926 , vol. 56, p. 764
Full Text Show Details
Higginbotham; Stephen
Journal of the Chemical Society, 1920 , vol. 117, p. 1541