1-甲氧基-4-(2-甲基-2-丙烯-1-基)苯合成路线 （共 18 条）
反应条件
caesium carbonate; palladium diacetate; tri-cyclo-hexyl-phosphine in toluene
24 h; Heating;
参考文献
Iwasaki, Masayuki; Hayashi, Sayuri; Hirano, Koji; Yorimitsu, Hideki; Oshima, Koichiro
Journal of the American Chemical Society, 2007 , vol. 129, # 14 p. 4463 - 4469
反应条件
caesium carbonate; tri-cyclo-hexyl-phosphine; palladium diacetate in N,N-dimethyl-formamide; toluene
T=250°C; 0.25 h; microwave irradiation;
参考文献
Iwasaki, Masayuki; Hayashi, Sayuri; Hirano, Koji; Yorimitsu, Hideki; Oshima, Koichiro
Tetrahedron, 2007 , vol. 63, # 24 p. 5200 - 5203
反应条件
Fe(acac)3 in tetrahydrofuran
T=25°C; 3 h; Inert atmosphere;
参考文献
Volla, Chandra M. R.; Markovic, Dean; Dubbaka, Srinivas Reddy; Vogel, Pierre
European Journal of Organic Chemistry, 2009 , # 36 p. 6281 - 6288
反应条件
pyridine; NiI2; 4-chloro-2-(4,5-dihydro-1H-imidazol-2-yl)pyridine; tetrabutylammomium bromide; magnesium chloride; zinc in N,N-dimethyl acetamide
T=60°C; 12 h; Schlenk techniqueInert atmosphere; regioselective reaction;
参考文献
Cui, Xiaozhan; Wang, Shulin; Zhang, Yuwei; Deng, Wei; Qian, Qun; Gong, Hegui
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 19 p. 3094 - 3097
反应条件
palladium diacetate; caesium carbonate; tris(4-methylphenyl)-phosphine in toluene
8 h; Heating;
参考文献
Hayashi, Sayuri; Hirano, Koji; Yorimitsu, Hideki; Oshima, Koichiro
Journal of the American Chemical Society, 2006 , vol. 128, # 7 p. 2210 - 2211
反应条件
palladium diacetate; caesium carbonate; tris(4-methylphenyl)-phosphine in toluene
8 h; Heating;
参考文献
Hayashi, Sayuri; Hirano, Koji; Yorimitsu, Hideki; Oshima, Koichiro
Journal of the American Chemical Society, 2006 , vol. 128, # 7 p. 2210 - 2211
反应条件
titanium tetrachloride; magnesium in tetrahydrofuran
T=0 - 20°C; 1.16667 h;
参考文献
Sadeghian, Hamid; Attaran, Neda; Jafari, Zeinab; Saberi, Mohammad Reza; Pordel, Mehdi; Riazi, Mohammad Mahdi
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 6 p. 2327 - 2335
反应条件
palladium (II) trifluoroacetate; potassium hydroxide in water
T=90°C; Suzuki Coupling; 3 h; Green chemistry;
参考文献
Dong, Chaonan; Zhang, Lingjuan; Xue, Xiao; Li, Huanrong; Yu, Zhiyong; Tang, Weijun; Xu, Lijin
RSC Advances, 2014 , vol. 4, # 22 p. 11152 - 11158
反应条件
copper(l) iodide in tetrahydrofuran
T=70°C; 1 h; Inert atmosphere; regioselective reaction;
参考文献
Li, Man-Bo; Tang, Xiang-Ling; Tian, Shi-Kai
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 1980 - 1984
反应条件
1: para-iodoanisole With chloro-trimethyl-silane; zinc in diethylene glycol dimethyl ether
T=130°C; 24 h;
2: 3-bromo-2-methylprop-1-ene With bis(dibenzylideneacetone)-palladium(0) in diethylene glycol dimethyl ether
T=0°C; 0.166667 h;
参考文献
Ikegami, Ryo; Koresawa, Akiko; Shibata, Takanori; Takagi, Kentaro
Journal of Organic Chemistry, 2003 , vol. 68, # 6 p. 2195 - 2199
