1-氯-4-(硫氰酸基甲基)苯合成路线 （共 15 条）
反应条件
1: Ammonium thiocyanate With selectfluor in acetonitrile T=20°C; 0.333333 h; 2: 4-chloro-1-hydroxymethyl-benzene in acetonitrile 0.5 h;
参考文献
Khazaei, Ardeshir; Rahmati, Sadegh; Khalafi-Nezhad, Ali; Saednia, Shahnaz
Journal of Fluorine Chemistry, 2012 , vol. 137, p. 123 - 125
反应条件
bromine; triphenylphosphine in acetonitrile T=20°C; Thiocyanation;
参考文献
Iranpoor; Firouzabadi; Shaterian
Journal of Chemical Research - Part S, 1999 , # 11 p. 676 - 677
反应条件
T=90°C; 0.0833333 h; Neat (no solvent)Grinding;
参考文献
Mokhtari, Babak; Azadi, Roya; Mardani, Edris
Tetrahedron Letters, 2012 , vol. 53, # 5 p. 491 - 493
反应条件
1: ammonium thiocyanate With bromine; triphenylphosphine in acetonitrile T=20°C; Addition; 2: 4-Cl-C6H4CH2OTMS in acetonitrile T=20°C; Substitution;
参考文献
Iranpoor; Firouzabadi; Shaterian
Synlett, 2000 , # 1 p. 65 - 66
反应条件
1: ammonium thiocyanate With PPh3.Br2 in acetonitrile T=20°C; 2: p-(Cl)C6H4CH2OTHP in acetonitrile T=20°C;
参考文献
Iranpoor, Nasser; Firouzabadi, Habib; Shaterian, Hamid Reza
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 9 p. 2093 - 2096
反应条件
poly(vinylbenzyltriphenylphosphonium chloride) in dichloromethane 3 h; Ambient temperature;
参考文献
Hassanein; Akelah; Selim; El-Hamshary
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 8 p. 763 - 765
反应条件
ammonium thiocyanate in acetonitrile T=20°C; 1 h;
参考文献
Mokhtari, Babak; Azadi, Roya; Rahmani-Nezhad, Samira
Tetrahedron Letters, 2009 , vol. 50, # 47 p. 6588 - 6589
参考文献
Molina, P.; Alajarin, M.; Ferao, A.; Lidon, M. J.; Fresneda, P. M.; Vilaplana, M. J.
Synthesis, 1982 , # 6 p. 472 - 475
反应条件
1: 91 percent / acetonitrile / 12 h / Ambient temperature 2: 54 percent / 180 °C View Scheme
参考文献
Molina, P.; Alajarin, M.; Ferao, A.; Lidon, M. J.; Fresneda, P. M.; Vilaplana, M. J.
Synthesis, 1982 , # 6 p. 472 - 475
反应条件
1.1: sodium tetrahydroborate; 1-n-butyl-3-methylimidazolium tetrafluoroborate / 20 °C 2.1: iodine; 1-n-butyl-3-methylimidazolium tetrafluoroborate / 0.5 h / 20 °C 2.2: 20 °C View Scheme
参考文献
Yadav, Lal Dhar S.; Garima; Kapoor, Ritu
Synthetic Communications, 2011 , vol. 41, # 1 p. 100 - 112
