4-甲氧基-2,6-二甲基吡啶合成路线 （共 9 条）
反应条件
triphenylphosphine in 1,2-bis-(2-hydroxyethoxy)-ethane T=200°C; 1 h; Inert atmosphere;
参考文献
Zohuri, Gholam Hossein; Seyedi, Seyed Mohammad; Sandaroos, Reza; Damavandi, Saman; Mohammadi, Ali
Catalysis Letters, 2010 , vol. 140, # 3-4 p. 160 - 166
反应条件
1: methanol 2: platinum /palladium/charcoal; acetic acid anhydride / Hydrogenation View Scheme
参考文献
Zohuri, Gholam Hossein; Seyedi, Seyed Mohammad; Sandaroos, Reza; Damavandi, Saman; Mohammadi, Ali
Catalysis Letters, 2010 , vol. 140, # 3-4 p. 160 - 166
反应条件
1: dihydrogen peroxide; acetic acid / water / 27 h / 70 °C / Inert atmosphere 2: sulfuric acid; nitric acid / 7 h / 128 - 130 °C / Inert atmosphere 3: methanol / 5 h / Reflux; Inert atmosphere 4: triphenylphosphine / 1,2-bis-(2-hydroxyethoxy)-ethane / 1 h / 200 °C / Inert atmosphere View Scheme
参考文献
Zohuri, Gholam Hossein; Seyedi, Seyed Mohammad; Sandaroos, Reza; Damavandi, Saman; Mohammadi, Ali
Catalysis Letters, 2010 , vol. 140, # 3-4 p. 160 - 166
反应条件
1: sulfuric acid; nitric acid / 7 h / 128 - 130 °C / Inert atmosphere 2: methanol / 5 h / Reflux; Inert atmosphere 3: triphenylphosphine / 1,2-bis-(2-hydroxyethoxy)-ethane / 1 h / 200 °C / Inert atmosphere View Scheme
参考文献
Zohuri, Gholam Hossein; Seyedi, Seyed Mohammad; Sandaroos, Reza; Damavandi, Saman; Mohammadi, Ali
Catalysis Letters, 2010 , vol. 140, # 3-4 p. 160 - 166
参考文献
Conrad; Eckhardt
Chemische Berichte, 1889 , vol. 22, p. 81
参考文献
Baeyer
Chemische Berichte, 1910 , vol. 43, p. 2338
参考文献
Baeyer
Chemische Berichte, 1910 , vol. 43, p. 2338
反应条件
2: silver oxide; water
View Scheme
参考文献
Conrad; Eckhardt
Chemische Berichte, 1889 , vol. 22, p. 81
反应条件
potassium permanganate
Inert atmosphere;
参考文献
Zohuri, Gholam Hossein; Seyedi, Seyed Mohammad; Sandaroos, Reza; Damavandi, Saman; Mohammadi, Ali
Catalysis Letters, 2010 , vol. 140, # 3-4 p. 160 - 166
