反应条件
N,N,N',N,-tetramethylethylenediamine; iodine in tetrahydrofuran Kinetics; to a soln. of nucleophile in THF was added soln. of complex in THF at -60°C; after 45 min at -60°C I2 in THF was added and soln. allowed to stir overnight while being warmed to room temp.;; soln. was filtered through Celite, evapd., extd. with ether, extract was washed with other solvents, then chromd. on silica column, eluent CHCl3-hexane;;
参考文献
Organometallics, , vol. 6, p. 242 - 249
