三甲基硅烷基4-甲氧基苯甲酸酯合成路线 (共 9 条)
反应条件
in diethyl ether T=20 - 25°C; 1 h;
参考文献
Anders, Ernst; Stankowiak, Achim; Riemer, Roland
Synthesis, 1987 , # 10 p. 931 - 934
反应条件
methyl iodide in toluene T=100 - 115°C; 40 h;
参考文献
Yamamoto, Yasushi; Shimizu, Hideaki; Hamada, Yoshitaka
Journal of Organometallic Chemistry, 1996 , vol. 509, # 2 p. 119 - 122
反应条件
1: [bis(acetoxy)iodo]benzene; Fe(TAML)Li; diphenylether; water / acetone / 1 h / 25 °C / |Green chemistry 2: 25 °C View Scheme
参考文献
Napoly, Francois; Jean-Gerard, Ludivine; Goux-Henry, Catherine; Draye, Micheline; Andrioletti, Bruno
European Journal of Organic Chemistry, 2014 , vol. 2014, # 4 p. 781 - 787
反应条件
1: 4-methoxy-benzoic acid With cytochrome P450 enzyme CYP199A4 from Rhodopseudomonas palustris HaA2; nicotinamide adenine dinucleotide; bovine liver catalase in ethanol pH=7.4; Enzymatic reaction; 2: N,O-bis(trimethylsilyl) trifluoroacetamide With chloro-trimethyl-silane in acetonitrile 2 h;
参考文献
Bell, Stephen G.; Zhou, Ruimin; Yang, Wen; Tan, Adrian B. H.; Gentleman, Alexander S.; Wong, Luet-Lok; Zhou, Weihong
Chemistry - A European Journal, 2012 , vol. 18, # 52 p. 16677 - 16688
参考文献
Napoly, Francois; Jean-Gerard, Ludivine; Goux-Henry, Catherine; Draye, Micheline; Andrioletti, Bruno
European Journal of Organic Chemistry, 2014 , vol. 2014, # 4 p. 781 - 787
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=-20°C; 1 h;
参考文献
Larson, Gerald L.; Ortiz, Margarita; Roca, Marisol Rodriguez de
Synthetic Communications, 1981 , vol. 11, # 7 p. 583 - 590
反应条件
water 0.5 h; Yield given;
参考文献
Yamamoto, Yasushi; Shimizu, Hideaki; Hamada, Yoshitaka
Journal of Organometallic Chemistry, 1996 , vol. 509, # 2 p. 119 - 122
反应条件
lithium aluminium tetrahydride in tetrahydrofuran T=-20°C; 1 h;
参考文献
Larson, Gerald L.; Ortiz, Margarita; Roca, Marisol Rodriguez de
Synthetic Communications, 1981 , vol. 11, # 7 p. 583 - 590
反应条件
XeF2 in dichloromethane
3 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Nongkunsarn, Pakawan; Ramsden, Christopher A.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 2 p. 121 - 122