4-(1-环己烯-1-基)-苯甲醚合成路线 （共 14 条）
反应条件
1: n-BuONO / HCl / acetic acid / 2 h / -10 °C 2: 55 percent / pyridine / 0.17 h / 70 °C 3: 43 percent / HCl / acetic acid; acetic anhydride / 2 h / 100 °C View Scheme
参考文献
Sivasubramanian, S.; Muthusubramanian, S.; Ramasamy, S.; Arumugam, N
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 7 p. 552 - 554
反应条件
1: trimethylsilyl cyanide With trifluorormethanesulfonic acid in 2,3,4-trifluorotoluene T=-20°C; 0.0833333 h; Inert atmosphere; 2: 4'-methoxy-2,3,4,5-tetrahydro-1,1'-biphenyl in 2,3,4-trifluorotoluene T=-20 - -5°C; Inert atmosphere;
参考文献
Yanagisawa, Arata; Nezu, Tetsuya; Mohri, Shin-Ichiro
Organic Letters, 2009 , vol. 11, # 22 p. 5286 - 5289
反应条件
chromium(VI) oxide; acetic acid
参考文献
Fieser; Szmuszkovicz
Journal of the American Chemical Society, 1948 , vol. 70, p. 3352,3354
反应条件
1: 1.) sodium borohydride, boron trifluoride etherate, 2.) 2 M aq. NaOH, 30percent aq. H2O2 / 1.) diglyme, THF, 3.5 h, 2.) diglyme, THF, ethanol, reflux, 1.7 h 2: 0.95 g / Jones reagent / acetone / 1 h View Scheme
参考文献
Collins, David J.; Molinski, Tadeusz F.; Sjoevall, Jan
Australian Journal of Chemistry, 1983 , vol. 36, # 2 p. 361 - 370
参考文献
Fieser; Szmuszkovicz
Journal of the American Chemical Society, 1948 , vol. 70, p. 3352,3354
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical; trimethylsilylazide; oxygen in acetonitrile T=80°C; P=760.051 Torr; 36 h; Schlenk technique; regioselective reaction;
参考文献
Wang, Teng; Jiao, Ning
Journal of the American Chemical Society, 2013 , vol. 135, # 32 p. 11692 - 11695
反应条件
in dimethyl sulfoxide Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Sivasubramanian; Aravind; Muthusubramanian
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1989 , vol. 28, # 12 p. 1005 - 1006
反应条件
1,1,2,2-tetramethylethylene; oxygen in acetonitrile T=20°C; 20 h; Irradiation400 W high-pressure mercury lamp; Yield given. Yields of byproduct given;
参考文献
Kojima, Masanobu; Sakuragi, Hirochika; Tokumaru, Katsumi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 9 p. 3331 - 3336
反应条件
1.1: BH3 / tetrahydrofuran / 2 h / 0 - 25 °C
1.2: aq. H2O2; aq. NaOH / tetrahydrofuran
2.1: PCC / CH2Cl2 / 8 h / 25 °C
View Scheme
参考文献
Collins, David J.; Molinski, Tadeusz F.; Sjoevall, Jan
Australian Journal of Chemistry, 1983 , vol. 36, # 2 p. 361 - 370
反应条件
diethyl ether
T=-20°C; Erhitzen des Reaktionsgemisches mit Ameisensaeure;
参考文献
Goldschmidt; Veer
Recueil des Travaux Chimiques des Pays-Bas, 1948 , vol. 67, p. 489,506
