2-甲基-5-苯基-2H-四唑合成路线 （共 28 条）
反应条件
potassium hydroxide in tetrahydrofuran; methanol; water T=20°C; Overall yield = 97 percent; Overall yield = 232 mg;
参考文献
Mastronardi, Federica; Gutmann, Bernhard; Oliver Kappe
Organic Letters, 2013 , vol. 15, # 21 p. 5590 - 5593
反应条件
sodium hydroxide; acetone
参考文献
Henry
Journal of the American Chemical Society, 1951 , vol. 73, p. 4470
反应条件
in toluene Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Boivin, Jean; Henriet, Eric; Zard, Samir Z.
Journal of the American Chemical Society, 1994 , vol. 116, # 21 p. 9739 - 9740
反应条件
sodium hydroxide; tetrabutylammomium bromide in dichloromethane T=25°C; 5 h; without solvent or tetrabutylammonium bromide; Product distribution;
参考文献
Spear, Robert J.
Australian Journal of Chemistry, 1984 , vol. 37, # 12 p. 2453 - 2468
反应条件
sodium hydroxide; tetrabutylammomium bromide in dichloromethane T=25°C; 5 h; without solvent or tetrabutylammonium bromide; Product distribution;
参考文献
Osipova, T. F.; Ostrovskii, V. A.; Koldobskii, G. I.; Erusalimskii, G. B.
Journal of Organic Chemistry USSR (English Translation), 1984 , vol. 20, p. 357 - 362
Zhurnal Organicheskoi Khimii, 1984 , vol. 20, # 2 p. 398 - 404
反应条件
in acetonitrile T=20°C; various temperatures: 10 deg. C, 15 deg. C, 25 deg. C, 30 deg. C, 35 deg. C; ΔH(excit), ΔS(excit);; Product distributionRate constantThermodynamic data;
参考文献
Agarkova, L.N.; Ostrovskii, V.A.; Koldobskii, G.I.; Erusalimskii, G.B.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 903 - 906
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 5 p. 1043 - 1047
参考文献
Lossen,W.; Statius
Justus Liebigs Annalen der Chemie, 1897 , vol. 298, p. 91
反应条件
triethylamine; dimethyl sulfate in chloroform T=40°C; 4 h; Microwave irradiation; Reactivity; Solvent;
参考文献
Efimova; Artamonova; Koldobskii
Russian Journal of Organic Chemistry, 2009 , vol. 45, # 5 p. 725 - 727
反应条件
in acetonitrile T=20°C; various temperatures: 10 deg. C, 15 deg. C, 25 deg. C, 30 deg. C, 35 deg. C; ΔH(excit), ΔS(excit);; Product distributionRate constantThermodynamic data;
参考文献
Agarkova, L.N.; Ostrovskii, V.A.; Koldobskii, G.I.; Erusalimskii, G.B.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 903 - 906
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 5 p. 1043 - 1047
反应条件
in acetonitrile T=20°C; various temperatures: 10 deg. C, 15 deg. C, 25 deg. C; ΔH(excit), ΔS(excit);; Product distributionRate constantThermodynamic data;
参考文献
Agarkova, L.N.; Ostrovskii, V.A.; Koldobskii, G.I.; Erusalimskii, G.B.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 903 - 906
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 5 p. 1043 - 1047
