N-Boc-内-3-氨基托烷合成路线 (共 4 条)
反应条件
palladium(II) hydroxide/carbon; ammonium formate in ethanol T=50°C; 7 h; Inert atmosphere;
参考文献
Journal of Medicinal Chemistry, , vol. 51, # 20 p. 6538 - 6546
反应条件
1: With ammonium formate; palladium 10 on activated carbon in methanol; water 2: With phosphoric acid in methanol; water pH=2; 3: With sodium hydroxide in methanol; water pH=12;
参考文献
US2006/100426 A1, ;
Page/Page column 18-19 ;
US 20060100426 A1
反应条件
water; ammonium formate; palladium 10 on activated carbon in methanol
参考文献
US2006/199839 A1, ;
Page/Page column 23-24 ;
US 20060199839 A1