1-羟基-3-甲氧基-9,10-蒽醌合成路线 （共 8 条）
反应条件
AlCl3, aluminium chloride; sodium chloride
T=165 - 175°C; Friedel-Crafts Acylation;
参考文献
Akhtar, Muhammad Nadeem; Zareen, Seema; Yeap, Swee Keong; Ho, Wan Yong; Lo, Kong Mun; Hasan, Aurangzeb; Alitheen, Noorjahan Banu
Molecules, 2013 , vol. 18, # 8 p. 10042 - 10055
反应条件
in neat (no solvent)
Ambient temperature;
参考文献
Savard, Jacques; Brassard, Paul
Tetrahedron, 1984 , vol. 40, # 18 p. 3455 - 3464
反应条件
potassium hydroxide
T=120°C;
参考文献
Plath
Chemische Berichte, 1876 , vol. 9, p. 1204
反应条件
triethylamine
1.) benzene, r.t., 120 h; 2.) reflux, 40 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Iwao, Masatomo; Kuraishi, Tsukasa
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 11 p. 4051 - 4060
反应条件
triethylamine
1.) toluene, 0 deg C, 0.5 h; 2.) 0 deg C, 6 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Iwao, Masatomo; Kuraishi, Tsukasa
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 11 p. 4051 - 4060
反应条件
triethylamine
1.) toluene, 0 deg C, 0.5 h; 2.) 0 deg C, 6 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Iwao, Masatomo; Kuraishi, Tsukasa
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 11 p. 4051 - 4060
参考文献
Graebe; Bernhard
Justus Liebigs Annalen der Chemie, 1906 , vol. 349, p. 227
参考文献
Fester; Suarez; Huck
Rev.fac.Quim.santa Fe, 1945 , vol. 14, p. 163,166
