(R)-(-)-扁桃酸甲酯合成路线 (共 107 条)
反应条件
in acetonitrile T=20°C; 6 h;
参考文献
Erb, Bernhard; Kucma, Jean-Philippe; Mourey, Sandrine; Struber, Fritz
Chemistry - A European Journal, 2003 , vol. 9, # 11 p. 2582 - 2588
反应条件
hydrogenchloride; sodium borohydride; sodium chloride in tetrahydrofuran
反应条件
FeCl2*4H2O; C35H30N2O2; sodium tetrakis[3,5-bis(trifluoromethyl)phenyl]borate; water in chloroform T=40°C; 10 h; Inert atmosphere; optical yield given as percent ee;
参考文献
Zhu, Shou-Fei; Cai, Yan; Mao, Hong-Xiang; Xie, Jian-Hua; Zhou, Qi-Lin
Nature Chemistry, 2010 , vol. 2, # 7 p. 546 - 551
反应条件
hydrogenchloride in diethyl ether T=4°C; 12 h;
参考文献
Tanaka, Kenzo; Mori, Atsunori; Inoue, Shohei
Journal of Organic Chemistry, 1990 , vol. 55, # 1 p. 181 - 185
反应条件
sodium hypochlorite; 4-phenylpyridine-N-oxide; phosphate buffer; 5,5'-MeO-substituted (R,R)-(salen)Mn(III) in dichloromethane T=0°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 120, # 4 p. 708 - 714
反应条件
in diethyl ether Methylation;
参考文献
Barrow, Russell A.; Moore, Richard E.; Li, Lian-Hai; Tius, Marcus A.
Tetrahedron, 2000 , vol. 56, # 21 p. 3339 - 3351
参考文献
Meyers, A. I.; Brown, Jack D.
Journal of the American Chemical Society, 1987 , vol. 109, # 10 p. 3155 - 3156
反应条件
osmium(VIII) oxide; chiral diamine derived from L-tartaric acid in dichloromethane T=-100°C; Yield given;
参考文献
Chemistry Letters, , p. 131 - 134
反应条件
IL1; Lipase PS-C in di-isopropyl ether T=35°C; 48 h;
参考文献
Itoh, Toshiyuki; Matsushita, Yuichi; Abe, Yoshikazu; Han, Shi-Hui; Wada, Shohei; Hayase, Shuichi; Kawatsura, Motoi; Takai, Shigeomi; Morimoto, Minoru; Hirose, Yoshihiko
Chemistry - A European Journal, 2006 , vol. 12, # 36 p. 9228 - 9237
反应条件
1: KH / tetrahydrofuran 2: Mg(ClO4)2 / 96 h 3: methanol View Scheme
参考文献
Journal of the American Chemical Society, , vol. 109, # 10 p. 3155 - 3156