chlorine in neat (no solvent)
addn. of mixt. of B-compds. to NMR tube contg. freshly sublimed AlCl3, addn. of Cl2 gas, warmed from -190°C to room temp., kept for 7 d; not isolated; detected by NMR;
参考文献
Nam, Wonwoo; Onak, Thomas
Inorganic Chemistry, 1987 , vol. 26, p. 1581 - 1586
aluminium trichloride in neat (no solvent)
addn. of B-compds. to NMR tube contg. freshly sublimed AlCl3, addn. of C2H5Cl, sealed, warmed form -190°C to room temp., kept for 8 d; not isolated; detected by NMR;
参考文献
Nam, Wonwoo; Onak, Thomas
Inorganic Chemistry, 1987 , vol. 26, p. 1581 - 1586
