2-甲基萘并[2,1-D]恶唑合成路线 (共 9 条)
反应条件
in N,N-dimethyl-formamide T=130°C; 3 h; Product distribution / selectivity;
参考文献
WO2006/23763 A1, ;
Page/Page column 12; 14 ;
反应条件
diethyl chlorophosphate in toluene Beckmann rearrangement; 0.166667 h; Reflux;
参考文献
Synlett, , # 9 p. 1391 - 1393
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 1937 - 1940
反应条件
in N,N-dimethyl-formamide T=130°C; 3 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 47, # 11 p. 1861 - 1864
反应条件
1: polyphosphoric acid / 140 - 145 °C 2: 80 °C / 0.1 Torr View Scheme
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 1937 - 1940
反应条件
1: (i) (diazotization), aq. HCl, (ii) NaN3, NaOAc 2: polyphosphoric acid / 140 - 145 °C 3: 80 °C / 0.1 Torr View Scheme
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 1937 - 1940
参考文献
Journal of the Chemical Society [Section] C: Organic, , p. 1937 - 1940
反应条件
Reaktion ueber mehrere Stufen;
参考文献
Eastman Kodak Co.
Patent: US1939201 , 1932 ;
反应条件
in acetonitrile
15 h; Heating;
参考文献
Narayanan, Narasimhachari; Patonay, Gabor
Journal of Organic Chemistry, 1995 , vol. 60, # 8 p. 2391 - 2395