3,9-二苯基-2,4,8,10-四噁唑氮杂[5.5]十一烷合成路线 （共 11 条）
反应条件
carbon in benzene 1.5 h; Heating;
参考文献
Lizarzaburu, Mike E.; Jones, Ryan M.; Nantz, Michael H.; Kurth, Mark J.
Organic Preparations and Procedures International, 1999 , vol. 31, # 4 p. 440 - 442
反应条件
tetrachlorosilane in acetonitrile T=20°C;
参考文献
Firouzabadi, Habib; Iranpoor, Nasser; Hazarkhani, Hassan
Phosphorus, Sulfur and Silicon and the Related Elements, 2002 , vol. 177, # 12 p. 2847 - 2858
反应条件
N-bromosuccinmide in dichloromethane T=20°C; 14 h;
参考文献
Karimi, Babak; Hazarkhani, Hassan; Maleki, Jafar
Synthesis, 2005 , # 2 art. no. Z11504SS, p. 279 - 285
反应条件
tetrachlorosilane in acetonitrile T=20°C;
参考文献
Firouzabadi, Habib; Iranpoor, Nasser; Hazarkhani, Hassan
Phosphorus, Sulfur and Silicon and the Related Elements, 2002 , vol. 177, # 12 p. 2847 - 2858
反应条件
tetrachlorosilane in acetonitrile T=20°C;
参考文献
Firouzabadi, Habib; Iranpoor, Nasser; Hazarkhani, Hassan
Phosphorus, Sulfur and Silicon and the Related Elements, 2002 , vol. 177, # 12 p. 2847 - 2858
反应条件
iron(II) sulfate in toluene cyclocondensation; 0.8 h; Heating;
参考文献
Jin, Tong-Shou; Ma, Yan-Ran; Li, Tong-Shuang; Wang, Jian-Xin
Journal of Chemical Research - Part S, 1999 , # 4 p. 268 - 269
反应条件
hydrogenchloride T=25°C;
参考文献
Ashry, E. S. H. El; Kilany, Y. El; Hamid, H. Abdel; El-Zemity, S. R.; Boghdady, S.
Journal of Chemical Research, Miniprint, 2003 , # 1 p. 111 - 128
反应条件
camphor-10-sulfonic acid in acetonitrile
参考文献
Gardiner, John M; Mather, Paul; Morjan, Ramy; Pritchard, Robin G; Warren, John E; Cooper, Malcolm L; Ferwanah, Abd El-Rahman S; Abu-Tiem, Omar S
Tetrahedron Letters, 2002 , vol. 43, # 11 p. 2091 - 2094
反应条件
trichloroisocyanuric acid in dichloromethane T=20°C; 2 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 177, # 11 p. 2571 - 2577
反应条件
1: 92 percent / DIBAL-H / hexane; CH2Cl2 / 12 h / 20 °C
2: 95 percent / Et3N; DMAP / CH2Cl2 / 4 h / 20 °C
3: 96 percent / H2 / 10 percent Pd/C / ethyl acetate / 24 h / 20 °C
View Scheme
参考文献
Lizarzaburu, Mike E.; Jones, Ryan M.; Nantz, Michael H.; Kurth, Mark J.
Organic Preparations and Procedures International, 1999 , vol. 31, # 4 p. 440 - 442
