13-cis-Retinonitrile合成路线 （共 5 条）
反应条件
1: 75 percent / tBuOK / methanol / 48 h / 20 °C 2: piperidine; pyridine / Heating View Scheme
参考文献
Valla, Alain; Valla, Benoist; Le Guillou, Regis; Cartier, Dominique; Dufosse, Laurent; Labia, Roger
Helvetica Chimica Acta, 2007 , vol. 90, # 3 p. 512 - 520
反应条件
1: DIBAL-H / toluene / 0.5 h / 0 °C 2: 75 percent / tBuOK / methanol / 48 h / 20 °C 3: piperidine; pyridine / Heating View Scheme
参考文献
Valla, Alain; Valla, Benoist; Le Guillou, Regis; Cartier, Dominique; Dufosse, Laurent; Labia, Roger
Helvetica Chimica Acta, 2007 , vol. 90, # 3 p. 512 - 520
反应条件
toluene-4-sulfonic acid in toluene 0.166667 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Zakharova, N. I.; Gutnikova, N. P.; Bekker, A. R.; Filippova, T. M.; Miropol'skaya, M. A.; Samokhvalov, G. I.
Journal of Organic Chemistry USSR (English Translation), 1985 , vol. 21, p. 1870 - 1874
Zhurnal Organicheskoi Khimii, 1985 , vol. 21, # 10 p. 2043 - 2048
反应条件
in hexane Irradiation; Yield given. Yields of byproduct given;
参考文献
Rao, V. Jayathirtha; Fenstemacher, Roland J.; Liu, R. S. H.
Tetrahedron Letters, 1984 , vol. 25, # 11 p. 1115 - 1118
反应条件
in acetonitrile Irradiation; Yield given. Yields of byproduct given;
参考文献
Rao, V. Jayathirtha; Fenstemacher, Roland J.; Liu, R. S. H.
Tetrahedron Letters, 1984 , vol. 25, # 11 p. 1115 - 1118
