all-trans-Retinonitrile合成路线 （共 15 条）
反应条件
in acetonitrile Irradiation; Yield given. Yields of byproduct given;
参考文献
Rao, V. Jayathirtha; Fenstemacher, Roland J.; Liu, R. S. H.
Tetrahedron Letters, 1984 , vol. 25, # 11 p. 1115 - 1118
反应条件
1: DIBAL-H / toluene / 30 h / 0 °C 2: LiAlH4; TiCl3 / tetrahydrofuran / 20 °C View Scheme
参考文献
Valla, Alain; Valla, Benoist; Le Guillou, Regis; Cartier, Dominique; Dufosse, Laurent; Labia, Roger
Helvetica Chimica Acta, 2007 , vol. 90, # 3 p. 512 - 520
反应条件
diisobutylaluminium hydride in hexane; Petroleum ether T=-60 - -20°C; 1 h;
参考文献
Pardoen, J. A; Winkel, C; Mulder, P.P.J; Lugtenburg, J
Recueil: Journal of the Royal Netherlands Chemical Society, 1984 , vol. 103, # 4 p. 135 - 141
反应条件
diisobutylaluminium hydride in toluene T=0°C; 30 h;
参考文献
Valla, Alain; Valla, Benoist; Le Guillou, Regis; Cartier, Dominique; Dufosse, Laurent; Labia, Roger
Helvetica Chimica Acta, 2007 , vol. 90, # 3 p. 512 - 520
反应条件
1: 95 percent / Diisobuthylaluminium hydride / petroleum ether; hexane / 1 h / -60 - -20 °C 2: 98 percent / KCN, MnO2, AcOH / methanol / 12 h / Ambient temperature View Scheme
参考文献
Pardoen, J. A; Winkel, C; Mulder, P.P.J; Lugtenburg, J
Recueil: Journal of the Royal Netherlands Chemical Society, 1984 , vol. 103, # 4 p. 135 - 141
