all-trans-Retinonitrile合成路线 （共 15 条）
反应条件
[Ru2(p-PriC6H4Me)2(μ-Cl)Cl]2; 4 A molecular sieve in acetonitrile T=80°C; 0.166667 h;
参考文献
Yang, Soon Ha; Chang, Sukbok
Organic Letters, 2001 , vol. 3, # 26 p. 4209 - 4211
反应条件
ammonium heptamolybdate; ammonium hydroxide; dihydrogen peroxide; tetra-(n-butyl)ammonium iodide in tetrahydrofuran T=20°C; 24 h;
参考文献
Varga, M.; Khodonov, A. A.; Mitsner, B. I.; Evstigneeva, R. P.
Journal of Organic Chemistry USSR (English Translation), 1987 , vol. 23, # 5 p. 1014 - 1015
Zhurnal Organicheskoi Khimii, 1987 , vol. 23, # 5 p. 1123 - 1125
反应条件
1: 75 percent / tBuOK / methanol / 48 h / 20 °C 2: piperidine; pyridine / Heating View Scheme
参考文献
Helvetica Chimica Acta, , vol. 90, # 3 p. 512 - 520
反应条件
1: DIBAL-H / toluene / 0.5 h / 0 °C 2: 75 percent / tBuOK / methanol / 48 h / 20 °C 3: piperidine; pyridine / Heating View Scheme
参考文献
Helvetica Chimica Acta, , vol. 90, # 3 p. 512 - 520
反应条件
1: 80 percent / n-butyllithium / tetrahydrofuran; hexane / 1 h / 0 °C 2: 100 percent / 4-(dimethyilamino)pyridine / toluene / 20 h / Ambient temperature 3: 93 percent / DBN / toluene / 1.5 h / Heating View Scheme
参考文献
Recueil: Journal of the Royal Netherlands Chemical Society, , vol. 103, # 4 p. 135 - 141
反应条件
1: 100 percent / 4-(dimethyilamino)pyridine / toluene / 20 h / Ambient temperature 2: 93 percent / DBN / toluene / 1.5 h / Heating View Scheme
参考文献
Recueil: Journal of the Royal Netherlands Chemical Society, , vol. 103, # 4 p. 135 - 141
反应条件
toluene-4-sulfonic acid in toluene 0.166667 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 21, p. 1870 - 1874
Zhurnal Organicheskoi Khimii, , vol. 21, # 10 p. 2043 - 2048
反应条件
acetamide; ammonium acetate; acetic acid
反应条件
diisobutylaluminium hydride in toluene T=0°C; 30 h;
参考文献
Valla, Alain; Valla, Benoist; Le Guillou, Regis; Cartier, Dominique; Dufosse, Laurent; Labia, Roger
Helvetica Chimica Acta, 2007 , vol. 90, # 3 p. 512 - 520
反应条件
in hexane Irradiation; Yield given. Yields of byproduct given;
参考文献
Rao, V. Jayathirtha; Fenstemacher, Roland J.; Liu, R. S. H.
Tetrahedron Letters, 1984 , vol. 25, # 11 p. 1115 - 1118
