反应条件
water in diethyl ether; water byproducts: HF; stirred for 2 h; sepn. of the ether layer, removal of solvent in vac., sublimation (110°C, 1E-1 Torr);
参考文献
Chisholm, Malcolm H.; Folting, Kirsten; Haubrich, Scott T.; Martin, James D.
Inorganica Chimica Acta, 1993 , vol. 213, p. 17 - 24