2'-羟基-4',5'-二甲氧基苯乙酮合成路线 (共 21 条)
反应条件
boron trifluoride-diethyl ether complex in acetic acid
参考文献
American Cyanamid Company
Patent: US5681968 A1, 1997 ;
反应条件
boron trifluoride diethyl etherate T=80 - 90°C;
参考文献
Ploypradith, Poonsakdi; Jinaglueng, Wiyada; Pavaro, Chitkavee; Ruchirawat, Somsak
Tetrahedron Letters, 2003 , vol. 44, # 7 p. 1363 - 1366
反应条件
AlCl3, aluminium chloride T=135°C; Fries rearrangement; 0.5 h;
参考文献
Nolan, Karen A.; Doncaster, Jeremy R.; Dunstan, Mark S.; Scott, Katherine A.; Frenkel, A. David; Siegel, David; Ross, David; Barnes, John; Levy, Colin; Leys, David; Whitehead, Roger C.; Stratford, Ian J.; Bryce, Richard A.
Journal of Medicinal Chemistry, 2009 , vol. 52, # 22 p. 7142 - 7156
反应条件
potassium carbonate in acetone Reflux;
参考文献
Sheng, Rong; Lin, Xiao; Zhang, Jing; Chol, Kim Sun; Huang, Wenhai; Yang, Bo; He, Qiaojun; Hu, Yongzhou
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 18 p. 6692 - 6698
反应条件
aluminium trichloride in diethyl ether 48 h; Ambient temperature;
参考文献
Banerji, A.; Goomer, N. C.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 2 p. 144 - 146
反应条件
N-ethyl-N,N-diisopropylamine in methanol; acetonitrile T=20°C;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 20, # 13 p. 3872 - 3875
反应条件
methanol; sodium methylate
参考文献
Atti della Accademia Nazionale dei Lincei, Classe di Scienze Fisiche, Matematiche e Naturali, Rendiconti, , vol. <5> 20 II, p. 123
反应条件
hydrogenchloride; zinc(II) chloride und Erwaermen des Reaktionsprodukts mit Wasser;
参考文献
Journal of the Chemical Society, , p. 562,565
反应条件
aluminium trichloride 1.) dichloroethane, 20 deg C, overnight 2.) nitrobenzene, reflux, 1 h; Yield given. Multistep reaction;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 89, # 6 p. 459 - 485
参考文献
Journal of the American Chemical Society, , vol. 56, p. 237