1,3-二(4-甲基苯基)-1-丙酮合成路线 (共 10 条)
反应条件
AlCl3, aluminium chloride T=25 - 30°C; Friedel-Crafts Acylation; 4 h;
参考文献
Zhou, Yang; Li, Xinyao; Hou, Shili; Xu, Jiaxi
Journal of Molecular Catalysis A: Chemical, 2012 , vol. 365, p. 203 - 211
反应条件
sodium tetrahydroborate; nickel dichloride in methanol; water T=20°C; 2.5 h;
参考文献
Khurana, Jitender Mohan; Sharma, Purnima
Bulletin of the Chemical Society of Japan, 2004 , vol. 77, # 3 p. 549 - 552
反应条件
potassium carbonate 0.075 h; Microwave irradiationSonicationReflux;
参考文献
Tetrahedron Letters, , vol. 53, # 9 p. 1160 - 1162
反应条件
bismuth trifluoromethanesulphonate; malononitrile in dichloromethane T=20°C; 15 h; regioselective reaction;
参考文献
Shang, Jun-Yan; Li, Fei; Bai, Xing-Feng; Jiang, Jian-Xiong; Yang, Ke-Fang; Lai, Guo-Qiao; Xu, Li-Wen
European Journal of Organic Chemistry, 2012 , # 14 p. 2809 - 2815
反应条件
2,2'-azo-bisisobutyronitrile T=75°C;
参考文献
Journal of Organic Chemistry, , vol. 35, p. 3192 - 3195
反应条件
1: 87 percent / sodium borohydride; nickel(II) chloride hexahydrate / methanol; H2O / 2.5 h / 20 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 77, # 3 p. 549 - 552
反应条件
1: 87 percent / sodium borohydride; nickel(II) chloride hexahydrate / methanol; H2O / 2.5 h / 20 °C View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 77, # 3 p. 549 - 552
反应条件
2: hexane / 20 - 23 °C / Irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 35, p. 3192 - 3195
反应条件
2: hexane / 20 - 23 °C / Irradiation View Scheme
参考文献
Journal of Organic Chemistry, , vol. 35, p. 3192 - 3195
反应条件
1: sodium hydroxide / ethanol; water / 20 °C 2: potassium carbonate / 0.07 h / Microwave irradiation; Sonication; Reflux View Scheme
参考文献
Tetrahedron Letters, , vol. 53, # 9 p. 1160 - 1162