Indeno(1,2,3-De)Quinoline合成路线 （共 3 条）
反应条件
palladium diacetate; CsO2CCMe3; bis(1,1-diphenylphosphino)methane in N,N-dimethyl-formamide T=110°C; 60 h;
参考文献
Huang, Qinhua; Campo, Marino A.; Yao, Tuanli; Tian, Qingping; Larock, Richard C.
Journal of Organic Chemistry, 2004 , vol. 69, # 24 p. 8251 - 8257
反应条件
1: 63 percent / PPh3; DEAD / tetrahydrofuran / 4 h / 0 - 20 °C 2: 80 percent / ICl / CH2Cl2 / 1 h / -78 °C 3: 92 percent / NaOH; O2 / ethanol / 12 h / 50 °C / 760 Torr 4: 54 percent / 1,1-bis(diphenylphosphino)methane; CsO2CCMe3; Pd(OAc)2 / dimethylformamide / 60 h / 110 °C View Scheme
参考文献
Huang, Qinhua; Campo, Marino A.; Yao, Tuanli; Tian, Qingping; Larock, Richard C.
Journal of Organic Chemistry, 2004 , vol. 69, # 24 p. 8251 - 8257
反应条件
1: 63 percent / PPh3; DEAD / tetrahydrofuran / 4 h / 0 - 20 °C 2: 80 percent / ICl / CH2Cl2 / 1 h / -78 °C 3: 92 percent / NaOH; O2 / ethanol / 12 h / 50 °C / 760 Torr 4: 54 percent / 1,1-bis(diphenylphosphino)methane; CsO2CCMe3; Pd(OAc)2 / dimethylformamide / 60 h / 110 °C View Scheme
参考文献
Huang, Qinhua; Campo, Marino A.; Yao, Tuanli; Tian, Qingping; Larock, Richard C.
Journal of Organic Chemistry, 2004 , vol. 69, # 24 p. 8251 - 8257
