3-甲基-3-硝基-丁烷-2-醇合成路线 （共 6 条）
反应条件
potassium tert-butylate in acetonitrile; tert-butyl alcohol T=0 - 20°C; Henry reaction; 24 h;
参考文献
Crich, David; Ranganathan, Krishnakumar; Rumthao, Sochanchingwung; Shirai, Michio
Journal of Organic Chemistry, 2003 , vol. 68, # 5 p. 2034 - 2037
参考文献
E. I. Du Pont de Nemours and Company
Patent: US4581178 A1, 1986 ;
反应条件
water unter Zusatz eines Anionen-Austauschers und eines Kationen-Austauschers;
参考文献
Rohm and Haas Co.
Patent: US2736741 , 1951 ;
参考文献
Akhmetov,M.Kh. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1970 , p. 1555 - 1557
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1970 , p. 1649 - 1651
反应条件
1: Raney nickel; aqueous methanol / <45 / 29420.3 - 51485.6 Torr / Hydrogenation 2: sulfuric acid / Erhitzen des erhaltenen Esters mit wss.Natronlauge View Scheme
参考文献
Jones
Journal of Organic Chemistry, 1944 , vol. 9, p. 491
反应条件
in water T=25°C; pH 9.2-9.6; Equilibrium constant;
参考文献
Belikov,V.M. et al.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1969 , p. 1987 - 1991
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1969 , p. 2130 - 2135
