1-(3-丁烯-1-基)-4-甲氧基苯合成路线 (共 30 条)
反应条件
triphenyl phosphite; [RhCl(η2:η2-cycloocta-1,5-diene)]2; NaBARF in 1,2-dichloro-ethane 1 h; Reflux; regioselective reaction;
参考文献
Onodera, Gen; Yamamoto, Eriko; Tonegawa, Shota; Iezumi, Makoto; Takeuchi, Ryo
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 11-12 p. 2013 - 2021
反应条件
in tetrahydrofuran; diethyl ether T=20°C; 4 h; Inert atmosphere;
参考文献
Wang, Yu-Fei; Gao, Ya-Ru; Mao, Shuai; Zhang, Yan-Lei; Guo, Dong-Dong; Yan, Zhao-Lei; Guo, Shi-Huan; Wang, Yong-Qiang
Organic Letters, 2014 , vol. 16, # 6 p. 1610 - 1613
反应条件
InOTf in toluene T=-20 - 20°C; 14 h; Inert atmosphere;
参考文献
Dao, Hai Thanh; Schneider, Uwe; Kobayashi, Shu
Chemistry - An Asian Journal, 2011 , vol. 6, # 9 p. 2522 - 2529
反应条件
(1,2,3,4,5-pentamethyl-cyclopenta-2,4-dienylmethyl)PPh2; nickel dichloride in diethyl ether T=25°C; 3 h;
参考文献
Uemura, Minoru; Yorimitsu, Hideki; Oshima, Koichiro
Chemical Communications, 2006 , # 45 p. 4726 - 4728
反应条件
in liquid sulphur dioxide T=20°C; 185 h;
参考文献
Mayr, Herbert; Gorath, Gorden; Bauer, Bernhard
Angewandte Chemie, 1994 , vol. 106, # 7 p. 793 - 794
反应条件
HFSI in dichloromethane T=-78°C; 0.0833333 h;
参考文献
Kaur, Gurmeet; Kaushik, Monica; Trehan, Sanjay
Tetrahedron Letters, 1997 , vol. 38, # 14 p. 2521 - 2524
反应条件
indium in tetrahydrofuran T=20°C; 0.5 h;
参考文献
Ranu, Brindaban C.; Banerjee, Subhash; Adak, Laksmikanta
Tetrahedron Letters, 2007 , vol. 48, # 41 p. 7374 - 7379
反应条件
n-butyllithium in tetrahydrofuran T=-78°C; 0.5 h;
参考文献
Nishitani; Mimaki; Sato; Yamakawa
Chemical and Pharmaceutical Bulletin, 1992 , vol. 40, # 1 p. 288 - 290
反应条件
ammonium chloride in tetrahydrofuran
反应条件
1: in tetrahydrofuran T=20°C; 0.5 h; Inert atmosphere; 2: With phosphonic acid diethyl ester in tetrahydrofuran Inert atmosphere;
参考文献
Li, Ying; Hu, Yuan-Yuan; Zhang, Song-Lin
Chemical Communications, 2013 , vol. 49, # 90 p. 10635 - 10637