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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-异丙基苯乙烯
合成路线
（共 20 条）
2055-40-5
4-异丙基苯乙烯
→
反应条件
645-13-6
4'-异丙基苯乙酮
反应条件
perchloric acid; oxygen; palladium diacetate; p-benozquinone; sodium nitrite in methanol; water T=20°C; Wacker Oxidation; 5 h; Schlenk techniqueSealed tubeGreen chemistry;
参考文献
Zhang, Guofu; Xie, Xiaoqiang; Wang, Yong; Wen, Xin; Zhao, Yun; Ding, Chengrong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 18 p. 2947 - 2950
2055-40-5
4-异丙基苯乙烯
→
反应条件
10099-57-7
4-异丙基苯乙醇
反应条件
(i) dicyclohexylborane, THF, (ii) KOH, H2O, H2O2, (heating); Multistep reaction;
参考文献
Murphy,R.; Prager,R.H.
Journal of Organometallic Chemistry, 1978 , vol. 156, p. 133 - 147
2055-40-5
4-异丙基苯乙烯
→
反应条件
122-03-2
4-异丙基苯甲醛
反应条件
sodium periodate in water; ethyl acetate; acetonitrile T=0°C; 3.5 h;
参考文献
Vijay Kumar; Prakash Reddy; Sridhar; Srinivas; Rama Rao
Synlett, 2009 , # 5 p. 739 - 742
201230-82-2
+
2055-40-5
4-异丙基苯乙烯
→
反应条件
34291-99-1
+
7775-00-0
反应条件
[3-{(1−3-η3)-1,2,3-trimethylallyl}-1,2-(CH3)2-3,1,2-closo-RhC2B9H9]; hydrogen in carbon dioxide T=60°C; P=22801.5 Torr; 3 - 5 h; Autoclaveliquid CO2; Reagent/catalyst; regioselective reaction;
参考文献
Lyubimov, Sergey E.; Rastorguev, Eugenie A.; Lubentsova, Kseniya I.; Korlyukov, Alexander A.; Davankov, Vadim A.
Tetrahedron Letters, 2013 , vol. 54, # 9 p. 1116 - 1119
→
反应条件
2055-40-5
4-异丙基苯乙烯
反应条件
hydrogenchloride; carbon monoxide; palladium(II) chloride in tetrahydrofuran; water
参考文献
Universite d'Ottawa/University of Ottawa
Patent: EP305089 A1, 1989 ;
1475-10-1
→
反应条件
2055-40-5
4-异丙基苯乙烯
反应条件
potassium hydrogensulfate T=190°C; P=50 Torr;
参考文献
Kraakmann, P. A.; Nibbering, E. T. J.; Wolf, W. H. de; Bickelhaupt, F.
Tetrahedron, 1987 , vol. 43, # 21 p. 5109 - 5124
2065-66-9
+
122-03-2
4-异丙基苯甲醛
→
反应条件
2055-40-5
4-异丙基苯乙烯
反应条件
1: triphenyl-methyl-phosphonium iodide With potassium tert-butylate in tetrahydrofuran T=0°C; 1 h; Inert atmosphere; 2: [4-isopropylphenyl]methanone in tetrahydrofuran T=20°C; Inert atmosphere;
参考文献
Zhang, Guofu; Xie, Xiaoqiang; Wang, Yong; Wen, Xin; Zhao, Yun; Ding, Chengrong
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 18 p. 2947 - 2950
108-05-4
+
586-61-8
→
反应条件
2055-40-5
4-异丙基苯乙烯
反应条件
[2,2']bipyridinyl; tetra-n-butylammonium tetrafluoroborate; cobalt(II) dibromide in pyridine; acetonitrile T=20°C; Electrolysis;
参考文献
Gomes, Paulo; Gosmini, Corinne; Perichon, Jacques
Tetrahedron, 2003 , vol. 59, # 17 p. 2999 - 3002
645-13-6
4'-异丙基苯乙酮
→
反应条件
2055-40-5
4-异丙基苯乙烯
反应条件
1: 83 percent / NaBH4 / methanol 2: 90 percent / KHSO4 / 190 °C / 50 Torr View Scheme
参考文献
Kraakmann, P. A.; Nibbering, E. T. J.; Wolf, W. H. de; Bickelhaupt, F.
Tetrahedron, 1987 , vol. 43, # 21 p. 5109 - 5124
98-82-8
→
反应条件
2055-40-5
4-异丙基苯乙烯
反应条件
1: 20 percent / AlCl3 / CS2 2: 83 percent / NaBH4 / methanol 3: 90 percent / KHSO4 / 190 °C / 50 Torr View Scheme
参考文献
Kraakmann, P. A.; Nibbering, E. T. J.; Wolf, W. H. de; Bickelhaupt, F.
Tetrahedron, 1987 , vol. 43, # 21 p. 5109 - 5124
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