双(4-氯苯基)二硒化物合成路线 (共 39 条)
反应条件
sulfuric acid; N(Et)4ClO4 in water; acetonitrile T=65°C; 14 h; electrochemical oxidation;
参考文献
Tetrahedron Letters, , vol. 23, # 11 p. 1161 - 1164
参考文献
Morgan; Elliott
Proceedings of the Chemical Society, London, 1914 , vol. 30, p. 248
反应条件
polymer supported borohydride; (2,2′-bipyridine)nickel(II) dibromide in tetrahydrofuran T=65°C; Substitution; dehalogenation; 16 h;
参考文献
Millois; Diaz
Organic letters, 2000 , vol. 2, # 12 p. 1705 - 1708
反应条件
1: (4-ClPhSe)2 With InI; 1-n-butyl-3-methylimidazolium tetrafluoroborate T=20°C; 0.0833333 h; Inert atmosphere; 2: benzyl chloride T=20°C;
参考文献
Narayanaperumal, Senthil; Alberto, Eduardo E.; De Andrade, Fabiano Molinos; Lenardao, Eder J.; Taube, Paulo S.; Braga, Antonio L.
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 22 p. 4647 - 4650
反应条件
1: (4-ClPhSe)2 With zinc in acetonitrile T=65°C; 1 h; 2: benzyl bromide in water; acetonitrile T=65°C; 0.5 h;
参考文献
Movassagh, Barahman; Shamsipoor, Mojgan
Synlett, 2005 , # 1 art. no. D25704ST, p. 121 - 122
反应条件
samarium; cadmium (II) chloride in water; N,N-dimethyl-formamide T=20 - 50°C; 3.5 h;
参考文献
Zheng, Yunfa; Bao, Weiliang; Zhang, Yongmin
Synthetic Communications, 2000 , vol. 30, # 10 p. 1731 - 1736
反应条件
selenium; copper(II) oxide; potassium hydroxide in dimethyl sulfoxide
T=90°C; 0.5 h; Inert atmosphere; regioselective reaction;
参考文献
Singh, Devender; Deobald, Anna M.; Camargo, Leandro R.S.; Tabarelli, Greice; Rodrigues, Oscar E.D.; Braga, Antonio L.
Organic Letters, 2010 , vol. 12, # 15 p. 3288 - 3291
反应条件
selenium; 1,10-phenanthroline; CuCl2·2H2O; tetrabutyl ammonium fluoride; caesium carbonate in water
T=120°C; 24 h; Sealed tube;
参考文献
Li, Zhengkai; Ke, Fang; Deng, Hang; Xu, Hualong; Xiang, Haifeng; Zhou, Xiangge
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 18 p. 2943 - 2946
反应条件
NaBO3; acetic acid in ethanol
T=20°C; 2 h;
参考文献
McKillop; Koyuncu; Krief; Dumont; Renier; Trabelsi
Tetrahedron Letters, 1990 , vol. 31, # 35 p. 5007 - 5010
反应条件
[2,2']bipyridinyl; selenium; copper(l) iodide; sodium carbonate; magnesium in N,N-dimethyl-formamide
T=110°C; 65 h; Inert atmosphere;
参考文献
Taniguchi, Nobukazu
Tetrahedron, 2012 , vol. 68, # 51 p. 10510 - 10515,6