2-氨基-6-甲氧基嘌呤合成路线 （共 26 条）
反应条件
1: 90 percent / dimethylsulfoxide / 12 h / Ambient temperature 2: 88 percent / NaH / dimethylsulfoxide / 1.) r.t., 1 h, 2.) r.t., 12 h View Scheme
参考文献
Journal of the Chemical Society - Perkin Transactions 1, , # 3 p. 185 - 186
反应条件
in methanol T=20 - 80°C; 2 h;
参考文献
Sakakibara, Norikazu; Tsukamoto, Ikuko; Tsuruta, Takashi; Takata, Maki; Konishi, Ryoji; Maruyama, Tokumi
Heterocycles, 2012 , vol. 85, # 5 p. 1105 - 1116
反应条件
sodium methylate in methanol 18 h; Heating;
参考文献
Watkins, Bruce E.; Rapoport, Henry
Journal of Organic Chemistry, 1982 , vol. 47, # 23 p. 4471 - 4477
反应条件
sodium hydride in dimethyl sulfoxide 1.) r.t., 1 h, 2.) r.t., 12 h;
参考文献
Lembicz, Nicola K.; Grant, Sharon; Clegg, William; Griffin, Roger J.; Heath, Sarah L.; Golding, Bernard T.
Journal of the Chemical Society - Perkin Transactions 1, 1997 , # 3 p. 185 - 186
反应条件
1: 85 percent / pyridine / 5 h / 0 - 20 °C 2: 85 percent / aq. NaOH / tetrahydrofuran; H2O / 6 h / Ambient temperature 3: 90 percent / tetrabutylammonium fluoride / tetrahydrofuran 4: 60 percent / sodium methoxide / methanol / 18 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 23 p. 4471 - 4477
反应条件
1: 90 percent / tetrabutylammonium fluoride / tetrahydrofuran 2: 60 percent / sodium methoxide / methanol / 18 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 47, # 23 p. 4471 - 4477
反应条件
methyl iodide in N,N-dimethyl-formamide T=50°C; 17 h; Yield given;
参考文献
Kohda; Baba; Kawazoe
Tetrahedron Letters, 1987 , vol. 28, # 50 p. 6285-6288
反应条件
1: CH3I / dimethylformamide / 17 h / 50 °C 2: dimethylformamide / 17 h / 50 °C View Scheme
参考文献
Kohda; Baba; Kawazoe
Tetrahedron Letters, 1987 , vol. 28, # 50 p. 6285-6288
反应条件
in N,N-dimethyl-formamide T=50°C; 17 h; Product distribution;
参考文献
Kohda; Baba; Kawazoe
Tetrahedron Letters, 1987 , vol. 28, # 50 p. 6285-6288
反应条件
T=200°C; reduced pressure; Product distribution;
参考文献
Kohda; Baba; Kawazoe
Tetrahedron Letters, 1987 , vol. 28, # 50 p. 6285-6288
