4-溴-N,N-二乙基苯胺合成路线 （共 32 条）
反应条件
in N,N-dimethyl-formamide
Ambient temperature; Product distribution;
参考文献
Effenberger, Franz; Steinbach, Adalbert; Epple, Gerhard; Hanauer, Johann
Chemische Berichte, 1983 , vol. 116, # 11 p. 3539 - 3551
反应条件
rhodium(III) 5,10,15,20-tetra(p-sulfonatophenyl)porphyrin; oxygen in methanol; water
T=90°C; P=760.051 Torr; 22 h;
参考文献
Ling, Zhen; Yun, Lin; Liu, Lianghui; Wu, Bing; Fu, Xuefeng
Chemical Communications, 2013 , vol. 49, # 39 p. 4214 - 4216
参考文献
Saitoh, Terunobu; Ichikawa, Junji
Journal of the American Chemical Society, 2005 , vol. 127, # 27 p. 9696 - 9697
反应条件
nitromethane; 2-iodosylbenzoic acid; [14C]-Tetramethylammonium bromide in tetrahydrofuran
T=70°C; 3 h; regioselective reaction;
参考文献
Potturi, Hima K.; Gurung, Ras K.; Hou, Yuqing
Journal of Organic Chemistry, 2012 , vol. 77, # 1 p. 626 - 631
反应条件
in N,N-dimethyl-formamide
Ambient temperature; Product distribution;
参考文献
Effenberger, Franz; Steinbach, Adalbert; Epple, Gerhard; Hanauer, Johann
Chemische Berichte, 1983 , vol. 116, # 11 p. 3539 - 3551
反应条件
in ethanol
1.) r.t., 12 h, 2.) reflux, 1 h;
参考文献
Effenberger, Franz; Steinbach, Adalbert; Epple, Gerhard; Hanauer, Johann
Chemische Berichte, 1983 , vol. 116, # 11 p. 3539 - 3551
反应条件
1: (i) Mg, I2, THF, (ii) /BRN= 1900390/
2: diethyl ether
View Scheme
参考文献
Benn,M.H. et al.
Journal of the Chemical Society, 1961 , p. 2365 - 2375
反应条件
1: 4-(N,N-diethylamino)-bromobenzene With n-butyllithium in tetrahydrofuran; hexane
T=-78°C; 1 h; Inert atmosphere;
2: 2-isopropoxy-4,4,5,5-tetramethyl-1,3,2-dioxaborolane in tetrahydrofuran; hexane
T=20°C; 12 h; Inert atmosphere;
参考文献
Park, Byung Sun; El-deeb, Ibrahim M.; Yoo, Kyung Ho; Han, Dong Keun; Tae, Jin Sung; Lee, So Ha
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 11 p. 3629 - 3634
反应条件
in N,N-dimethyl-formamide
Ambient temperature; Product distribution;
参考文献
Effenberger, Franz; Steinbach, Adalbert; Epple, Gerhard; Hanauer, Johann
Chemische Berichte, 1983 , vol. 116, # 11 p. 3539 - 3551
反应条件
tetrabutyl ammonium fluoride; palladium dichloride; tri-cyclo-hexyl-phosphine in water; dimethyl sulfoxide
T=80°C; 3 h;
参考文献
Sahoo, Akhila K.; Oda, Takuro; Nakao, Yoshiaki; Hiyama, Tamejiro
Advanced Synthesis and Catalysis, 2004 , vol. 346, # 13-15 p. 1715 - 1727
